Synthesis, structure and electrochemical properties of 1-ferrocenyl-3-cymantrenyl-containing β-diketone, pyrazole and mixed-metal chelated complex of p-cymene-ruthenium-iodide
Publication type: Journal Article
Publication date: 2018-07-01
scimago Q3
wos Q2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract Claisen condensation of acetylferrocene (η5-C5H5)Fe(η5-C5H4COCH3) and methyl ether of cymantrenecarboxylic acid (CO)3Mn(η5-C5H4COOMe) results in β-diketone (η5-C5H5)Fe(η5-C5H4)-C(O)CH2C(O)-(η5-C5H4)Mn(CO)3 (I) which reacts with hydrazine to form a heterometallic pyrazole (η5-C5H5)Fe(η5-C5H4)-N2C3H3-(η5-C5H4)Mn(CO)3 (II) or reacts with diiodo(p-cymene)ruthenium(II) dimer giving chelate β-ketoenolate complexes of ruthenium, (p-cymene)RuI[(η5-C5H5)Fe(η5-C5H4)-C(O)CHC(O)-(η5-C5H4)Mn(CO)3] (III). The structures of complexes I–III were determined by single crystal X-ray diffraction. Electrochemical properties were studied too.
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Shapovalov S. S. et al. Synthesis, structure and electrochemical properties of 1-ferrocenyl-3-cymantrenyl-containing β-diketone, pyrazole and mixed-metal chelated complex of p-cymene-ruthenium-iodide // Polyhedron. 2018. Vol. 149. pp. 73-78.
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Shapovalov S. S., Tikhonova O. G., Kolos A. V., Pasynskii A. A., Skabitsky I. V., Denisov G. L., Grinberg V. A. Synthesis, structure and electrochemical properties of 1-ferrocenyl-3-cymantrenyl-containing β-diketone, pyrazole and mixed-metal chelated complex of p-cymene-ruthenium-iodide // Polyhedron. 2018. Vol. 149. pp. 73-78.
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TY - JOUR
DO - 10.1016/j.poly.2018.04.011
UR - https://doi.org/10.1016/j.poly.2018.04.011
TI - Synthesis, structure and electrochemical properties of 1-ferrocenyl-3-cymantrenyl-containing β-diketone, pyrazole and mixed-metal chelated complex of p-cymene-ruthenium-iodide
T2 - Polyhedron
AU - Shapovalov, Sergey S.
AU - Tikhonova, O G
AU - Kolos, A V
AU - Pasynskii, A. A.
AU - Skabitsky, I. V.
AU - Denisov, Gleb L
AU - Grinberg, V. A.
PY - 2018
DA - 2018/07/01
PB - Elsevier
SP - 73-78
VL - 149
SN - 0277-5387
SN - 1873-3719
ER -
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@article{2018_Shapovalov,
author = {Sergey S. Shapovalov and O G Tikhonova and A V Kolos and A. A. Pasynskii and I. V. Skabitsky and Gleb L Denisov and V. A. Grinberg},
title = {Synthesis, structure and electrochemical properties of 1-ferrocenyl-3-cymantrenyl-containing β-diketone, pyrazole and mixed-metal chelated complex of p-cymene-ruthenium-iodide},
journal = {Polyhedron},
year = {2018},
volume = {149},
publisher = {Elsevier},
month = {jul},
url = {https://doi.org/10.1016/j.poly.2018.04.011},
pages = {73--78},
doi = {10.1016/j.poly.2018.04.011}
}