volume 57 issue 3 pages 1656-1664

Steric and Acidity Control in Hydrogen Bonding and Proton Transfer to trans-W(N2)2(dppe)2

Nikolay V Kireev 1, 2, 3
Oleg A. Filippov 1, 3
Lina M. epstein 1, 3
Victor D Makhaev 4
Elena S. Shubina 1, 3
Publication typeJournal Article
Publication date2018-01-19
scimago Q1
wos Q1
SJR0.958
CiteScore7.4
Impact factor4.7
ISSN00201669, 1520510X
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The interaction of trans-W(N2)2(dppe)2 (1; dppe = 1,2-bis(diphenylphosphino)ethane) with relatively weak acids (p-nitrophenol, fluorinated alcohols, CF3COOH) was studied by means of variable temperature IR and NMR spectroscopy and complemented by DFT/B3PW91-D3 calculations. The results show, for the first time, the formation of a hydrogen bond to the coordinated dinitrogen, W-N≡N···H-O, that is preferred over H-bonding to the metal atom, W···H-O, despite the higher proton affinity of the latter. Protonation of the core metal-the undesirable side step in the conversion of N2 to NH3-can be avoided by using weaker and, more importantly, bulkier acids.
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Kireev N. V. et al. Steric and Acidity Control in Hydrogen Bonding and Proton Transfer to trans-W(N2)2(dppe)2 // Inorganic Chemistry. 2018. Vol. 57. No. 3. pp. 1656-1664.
GOST all authors (up to 50) Copy
Kireev N. V., Filippov O. A., Pavlov A., Pavlov A. A., epstein L. M., Makhaev V. D., Dyadchenko V. P., Shubina E. S., Belkova N. V. Steric and Acidity Control in Hydrogen Bonding and Proton Transfer to trans-W(N2)2(dppe)2 // Inorganic Chemistry. 2018. Vol. 57. No. 3. pp. 1656-1664.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/acs.inorgchem.7b03027
UR - https://pubs.acs.org/doi/10.1021/acs.inorgchem.7b03027
TI - Steric and Acidity Control in Hydrogen Bonding and Proton Transfer to trans-W(N2)2(dppe)2
T2 - Inorganic Chemistry
AU - Kireev, Nikolay V
AU - Filippov, Oleg A.
AU - Pavlov, Alexander
AU - Pavlov, Alexander A.
AU - epstein, Lina M.
AU - Makhaev, Victor D
AU - Dyadchenko, Victor P.
AU - Shubina, Elena S.
AU - Belkova, Natalia V
PY - 2018
DA - 2018/01/19
PB - American Chemical Society (ACS)
SP - 1656-1664
IS - 3
VL - 57
PMID - 29350026
SN - 0020-1669
SN - 1520-510X
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2018_Kireev,
author = {Nikolay V Kireev and Oleg A. Filippov and Alexander Pavlov and Alexander A. Pavlov and Lina M. epstein and Victor D Makhaev and Victor P. Dyadchenko and Elena S. Shubina and Natalia V Belkova},
title = {Steric and Acidity Control in Hydrogen Bonding and Proton Transfer to trans-W(N2)2(dppe)2},
journal = {Inorganic Chemistry},
year = {2018},
volume = {57},
publisher = {American Chemical Society (ACS)},
month = {jan},
url = {https://pubs.acs.org/doi/10.1021/acs.inorgchem.7b03027},
number = {3},
pages = {1656--1664},
doi = {10.1021/acs.inorgchem.7b03027}
}
MLA
Cite this
MLA Copy
Kireev, Nikolay V., et al. “Steric and Acidity Control in Hydrogen Bonding and Proton Transfer to trans-W(N2)2(dppe)2.” Inorganic Chemistry, vol. 57, no. 3, Jan. 2018, pp. 1656-1664. https://pubs.acs.org/doi/10.1021/acs.inorgchem.7b03027.