Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition
Aleksey A Nikitin
1, 2
,
Igor Shchetinin
1
,
Igor V. Shchetinin
1
,
Natalya Yu Tabachkova
1
,
Mikhail Soldatov
3
,
Alexander V. Soldatov
3
,
Natalya V Sviridenkova
1
,
Natalya D Fedorova
1
,
Maxim A. Abakumov
2, 4
,
Alexander G. Majouga
1, 2, 5
3
Publication type: Journal Article
Publication date: 2018-03-22
scimago Q1
wos Q2
SJR: 0.763
CiteScore: 6.0
Impact factor: 3.9
ISSN: 07437463, 15205827
PubMed ID:
29566327
Spectroscopy
Electrochemistry
Condensed Matter Physics
General Materials Science
Surfaces and Interfaces
Abstract
Herein, we report a novel one-step solvothermal synthesis of magnetite nanoclusters (MNCs). In this report, we discuss the synthesis, structure, and properties of MNCs and contrast enhancement in T2-weighted MR images using magnetite nanoclusters. The effect of different organic acids, used as surfactants, on the size and shape of MNCs was investigated. The structure and properties of samples were determined by magnetic measurements, TGA, TEM, HRTEM, XRD, FTIR, and MRI. Magnetic measurements show that obtained MNCs have relatively high saturation magnetization values (65.1-81.5 emu/g) and dependence of the coercive force on the average size of MNCs was established. MNCs were transferred into an aqueous medium by Pluronic F-127, and T2-relaxivity values were determined. T2-Weighted MR phantom images clearly demonstrated that such magnetite nanoclusters can be used as contrast agents for MRI.
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Metrics
34
Total citations:
34
Citations from 2024:
7
(20%)
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GOST
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Nikitin A. A. et al. Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition // Langmuir. 2018. Vol. 34. No. 15. pp. 4640-4650.
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Nikitin A. A., Shchetinin I., Shchetinin I. V., Tabachkova N. Yu., Soldatov M., Soldatov A., Soldatov A. V., Sviridenkova N. V., Beloglazkina E. K., Savchenko A. G., Fedorova N. D., Abakumov M. A., Majouga A. G. Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition // Langmuir. 2018. Vol. 34. No. 15. pp. 4640-4650.
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RIS
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TY - JOUR
DO - 10.1021/acs.langmuir.8b00753
UR - https://pubs.acs.org/doi/10.1021/acs.langmuir.8b00753
TI - Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition
T2 - Langmuir
AU - Nikitin, Aleksey A
AU - Shchetinin, Igor
AU - Shchetinin, Igor V.
AU - Tabachkova, Natalya Yu
AU - Soldatov, Mikhail
AU - Soldatov, Alexander
AU - Soldatov, Alexander V.
AU - Sviridenkova, Natalya V
AU - Beloglazkina, Elena K.
AU - Savchenko, Alexander G.
AU - Fedorova, Natalya D
AU - Abakumov, Maxim A.
AU - Majouga, Alexander G.
PY - 2018
DA - 2018/03/22
PB - American Chemical Society (ACS)
SP - 4640-4650
IS - 15
VL - 34
PMID - 29566327
SN - 0743-7463
SN - 1520-5827
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2018_Nikitin,
author = {Aleksey A Nikitin and Igor Shchetinin and Igor V. Shchetinin and Natalya Yu Tabachkova and Mikhail Soldatov and Alexander Soldatov and Alexander V. Soldatov and Natalya V Sviridenkova and Elena K. Beloglazkina and Alexander G. Savchenko and Natalya D Fedorova and Maxim A. Abakumov and Alexander G. Majouga},
title = {Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition},
journal = {Langmuir},
year = {2018},
volume = {34},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://pubs.acs.org/doi/10.1021/acs.langmuir.8b00753},
number = {15},
pages = {4640--4650},
doi = {10.1021/acs.langmuir.8b00753}
}
Cite this
MLA
Copy
Nikitin, Aleksey A., et al. “Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition.” Langmuir, vol. 34, no. 15, Mar. 2018, pp. 4640-4650. https://pubs.acs.org/doi/10.1021/acs.langmuir.8b00753.