Langmuir, volume 34, issue 15, pages 4640-4650

Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition

Tabachkova Natalya Yu 1
Sviridenkova Natalya V 1
Fedorova Natalya D 1
Publication typeJournal Article
Publication date2018-03-22
Journal: Langmuir
Quartile SCImago
Q1
Quartile WOS
Q2
Impact factor3.9
ISSN07437463, 15205827
Spectroscopy
Electrochemistry
Condensed Matter Physics
General Materials Science
Surfaces and Interfaces
Abstract
Herein, we report a novel one-step solvothermal synthesis of magnetite nanoclusters (MNCs). In this report, we discuss the synthesis, structure, and properties of MNCs and contrast enhancement in T2-weighted MR images using magnetite nanoclusters. The effect of different organic acids, used as surfactants, on the size and shape of MNCs was investigated. The structure and properties of samples were determined by magnetic measurements, TGA, TEM, HRTEM, XRD, FTIR, and MRI. Magnetic measurements show that obtained MNCs have relatively high saturation magnetization values (65.1-81.5 emu/g) and dependence of the coercive force on the average size of MNCs was established. MNCs were transferred into an aqueous medium by Pluronic F-127, and T2-relaxivity values were determined. T2-Weighted MR phantom images clearly demonstrated that such magnetite nanoclusters can be used as contrast agents for MRI.

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Nikitin A. A. et al. Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition // Langmuir. 2018. Vol. 34. No. 15. pp. 4640-4650.
GOST all authors (up to 50) Copy
Nikitin A. A., Shchetinin I., Tabachkova N. Yu., Soldatov M., Soldatov A., Sviridenkova N. V., Beloglazkina E. K., Savchenko A. G., Fedorova N. D., Abakumov M. A., Majouga A. G. Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition // Langmuir. 2018. Vol. 34. No. 15. pp. 4640-4650.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/acs.langmuir.8b00753
UR - https://doi.org/10.1021%2Facs.langmuir.8b00753
TI - Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition
T2 - Langmuir
AU - Tabachkova, Natalya Yu
AU - Sviridenkova, Natalya V
AU - Fedorova, Natalya D
AU - Nikitin, Aleksey A
AU - Soldatov, Mikhail
AU - Majouga, Alexander G.
AU - Shchetinin, Igor
AU - Soldatov, Alexander
AU - Beloglazkina, Elena K.
AU - Savchenko, Alexander G.
AU - Abakumov, Maxim A.
PY - 2018
DA - 2018/03/22 00:00:00
PB - American Chemical Society (ACS)
SP - 4640-4650
IS - 15
VL - 34
SN - 0743-7463
SN - 1520-5827
ER -
BibTex |
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BibTex Copy
@article{2018_Nikitin,
author = {Natalya Yu Tabachkova and Natalya V Sviridenkova and Natalya D Fedorova and Aleksey A Nikitin and Mikhail Soldatov and Alexander G. Majouga and Igor Shchetinin and Alexander Soldatov and Elena K. Beloglazkina and Alexander G. Savchenko and Maxim A. Abakumov},
title = {Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition},
journal = {Langmuir},
year = {2018},
volume = {34},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://doi.org/10.1021%2Facs.langmuir.8b00753},
number = {15},
pages = {4640--4650},
doi = {10.1021/acs.langmuir.8b00753}
}
MLA
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MLA Copy
Nikitin, Aleksey A., et al. “Synthesis of Iron Oxide Nanoclusters by Thermal Decomposition.” Langmuir, vol. 34, no. 15, Mar. 2018, pp. 4640-4650. https://doi.org/10.1021%2Facs.langmuir.8b00753.
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