Chemistry of Materials, volume 27, issue 7, pages 2246-2285
The heat-up synthesis of colloidal nanocrystals
Publication type: Journal Article
Publication date: 2015-04-03
Journal:
Chemistry of Materials
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 8.6
ISSN: 08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Abstract
The successful transition of any nanocrystal-based product from the research phase to the commercial arena hinges on the ability to produce the required nanomaterial on large scales. The synthesis of colloidal nanocrystals using a heat-up (non-injection) method is a reliable means to achieve high quality nanomaterials on large scales with little or no batch-to-batch variation. In this class of synthesis precursors are heated within a reaction medium to induce a chemical reaction that yields monomer for nucleation and growth. Use of the heat-up technique circumvents the pitfalls of mixing time and poor heat management inherent to classical “hot-injection” methods. In heat-up syntheses monomer is produced in a more continuous fashion during the heating stage, making it more difficult to separate the nucleation and growth stages of the reaction, a factor that is conventionally considered detrimental toward achieving homogeneous colloidal dispersions. However, through the judicious selection of precursors, st...
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Van Embden J., Chesman A., Jasieniak J. The heat-up synthesis of colloidal nanocrystals // Chemistry of Materials. 2015. Vol. 27. No. 7. pp. 2246-2285.
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Van Embden J., Chesman A., Jasieniak J. The heat-up synthesis of colloidal nanocrystals // Chemistry of Materials. 2015. Vol. 27. No. 7. pp. 2246-2285.
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TY - JOUR
DO - 10.1021/cm5028964
UR - https://doi.org/10.1021/cm5028964
TI - The heat-up synthesis of colloidal nanocrystals
T2 - Chemistry of Materials
AU - Van Embden, Joel
AU - Chesman, A.S.R.
AU - Jasieniak, Jacek
PY - 2015
DA - 2015/04/03 00:00:00
PB - American Chemical Society (ACS)
SP - 2246-2285
IS - 7
VL - 27
SN - 0897-4756
SN - 1520-5002
ER -
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@article{2015_Van Embden,
author = {Joel Van Embden and A.S.R. Chesman and Jacek Jasieniak},
title = {The heat-up synthesis of colloidal nanocrystals},
journal = {Chemistry of Materials},
year = {2015},
volume = {27},
publisher = {American Chemical Society (ACS)},
month = {apr},
url = {https://doi.org/10.1021/cm5028964},
number = {7},
pages = {2246--2285},
doi = {10.1021/cm5028964}
}
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Van Embden, Joel, et al. “The heat-up synthesis of colloidal nanocrystals.” Chemistry of Materials, vol. 27, no. 7, Apr. 2015, pp. 2246-2285. https://doi.org/10.1021/cm5028964.