Peculiarities of the Complexation of Copper and Silver Adducts of a 3,5-Bis(trifluoromethyl)pyrazolate Ligand with Organoiron Compounds
Тип публикации: Journal Article
Дата публикации: 2011-03-15
scimago Q1
wos Q1
БС1
SJR: 0.958
CiteScore: 7.4
Impact factor: 4.7
ISSN: 00201669, 1520510X
PubMed ID:
21405060
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
Interaction of the copper, {[3,5-(CF(3))(2)Pz]Cu}(3), and silver, {[3,5-(CF(3))(2)Pz]Ag}(3), macrocycles [3,5-(CF(3))(2)Pz = 3,5-bis(trifluoromethyl)pyrazolate] with cyclooctatetraeneiron tricarbonyl, (cot)Fe(CO)(3), was investigated by IR and NMR spectroscopy for the first time. The formation of 1:1 complexes was observed at low temperatures in hexane. The composition of the complexes (1:1) and their thermodynamic characteristics in hexane and dichloromethane were determined. The π-electron system of (cot)Fe(CO)(3) was proven to be the sole site of coordination in solution and in the solid state. However, according to the single-crystal X-ray data, the complex has a different (2:1) composition featuring the sandwich structure. The complexes of ferrocene with copper and silver macrocycles have a columnar structure (X-ray data).
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Tsupreva V. N. et al. Peculiarities of the Complexation of Copper and Silver Adducts of a 3,5-Bis(trifluoromethyl)pyrazolate Ligand with Organoiron Compounds // Inorganic Chemistry. 2011. Vol. 50. No. 8. pp. 3325-3331.
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Tsupreva V. N., Titov A. A., Filippov O. A., Bilyachenko A. N., Smol’yakov A. F., Dolgushin F., Agapkin D. V., Godovikov I. A., epstein L. M., Shubina E. S. Peculiarities of the Complexation of Copper and Silver Adducts of a 3,5-Bis(trifluoromethyl)pyrazolate Ligand with Organoiron Compounds // Inorganic Chemistry. 2011. Vol. 50. No. 8. pp. 3325-3331.
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TY - JOUR
DO - 10.1021/ic102132v
UR - https://doi.org/10.1021/ic102132v
TI - Peculiarities of the Complexation of Copper and Silver Adducts of a 3,5-Bis(trifluoromethyl)pyrazolate Ligand with Organoiron Compounds
T2 - Inorganic Chemistry
AU - Tsupreva, Victoria N
AU - Titov, Alexey A
AU - Filippov, Oleg A.
AU - Bilyachenko, Alexey N
AU - Smol’yakov, Alexander F.
AU - Dolgushin, Fedor
AU - Agapkin, Denis V
AU - Godovikov, Ivan A
AU - epstein, Lina M.
AU - Shubina, Elena S.
PY - 2011
DA - 2011/03/15
PB - American Chemical Society (ACS)
SP - 3325-3331
IS - 8
VL - 50
PMID - 21405060
SN - 0020-1669
SN - 1520-510X
ER -
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@article{2011_Tsupreva,
author = {Victoria N Tsupreva and Alexey A Titov and Oleg A. Filippov and Alexey N Bilyachenko and Alexander F. Smol’yakov and Fedor Dolgushin and Denis V Agapkin and Ivan A Godovikov and Lina M. epstein and Elena S. Shubina},
title = {Peculiarities of the Complexation of Copper and Silver Adducts of a 3,5-Bis(trifluoromethyl)pyrazolate Ligand with Organoiron Compounds},
journal = {Inorganic Chemistry},
year = {2011},
volume = {50},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://doi.org/10.1021/ic102132v},
number = {8},
pages = {3325--3331},
doi = {10.1021/ic102132v}
}
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MLA
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Tsupreva, Victoria N., et al. “Peculiarities of the Complexation of Copper and Silver Adducts of a 3,5-Bis(trifluoromethyl)pyrazolate Ligand with Organoiron Compounds.” Inorganic Chemistry, vol. 50, no. 8, Mar. 2011, pp. 3325-3331. https://doi.org/10.1021/ic102132v.
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