Bi- and Mononuclear Nickel(II) Trimethylacetate Complexes with Pyridine Bases as Ligands
Igor L. Eremenko
1
,
Sergei E Nefedov
1
,
Margarita A Golubnichaya
1
,
Pavel V. Danilov
1
,
Vladimir N Ikorskii
1
,
Yury G. Shvedenkov
1
,
Vladimir M. Novotortsev
1
,
Publication type: Journal Article
Publication date: 1999-07-29
scimago Q1
wos Q1
SJR: 0.958
CiteScore: 7.4
Impact factor: 4.7
ISSN: 00201669, 1520510X
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Reaction of the nine-nuclear cluster Ni9(HOOCCMe3)4(μ4-ΟΗ)3(μ3-OH)3 (OOCCMe3)12 (1) with pyridine results in the binuclear species Py4Ni2(OOCCMe3)2(μ-OOCCMe3)2(μ-OH2) (2). Thermolysis of 2 at 100−140 °C in toluene or xylene leads to complex Py2Ni2(HOOCCMe3)2(OOCCMe3)2(μ-OOCCMe3)2(μ-OH2) (3). This complex can be converted back in 2 by the reaction of 3 with 2 equiv of pyridine. Thermolysis of solid 3 in vacuo at 170 °C gives the binuclear tetra-bridged trimethylacetate Py2Ni2(μ-OOCCMe3)4 (4) which can be reverted in 3 by reaction with 1 equiv of H2O and 2 equiv of HOOCCMe3. Compound 4 might be also prepared by the reaction of the complexs L2Ni2(μ-OOCCMe3)4 (L = 2,3-lutidine (5), Et3N (6)) with pyridine at 40−80 °C in hexane or benzene solution. Complexes 5 and 6 are formed in an one-step reaction by interaction of complex 1 and ligand L. Complex Dipy2Ni2(OOCCMe3)2(μ-OOCCMe3)2(μ-OH2) (7), an isoelectronic analogue of complex 2, was prepared by reacting 1 with Dipy. Thermolysis of solid 7 at 170 °C in vacuo ...
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Eremenko I. L. et al. Bi- and Mononuclear Nickel(II) Trimethylacetate Complexes with Pyridine Bases as Ligands // Inorganic Chemistry. 1999. Vol. 38. No. 17. pp. 3764-3773.
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Eremenko I. L., Nefedov S. E., Sidorov A. A., Golubnichaya M. A., Danilov P. V., Ikorskii V. N., Shvedenkov Y. G., Novotortsev V. M., Moiseev I. I. Bi- and Mononuclear Nickel(II) Trimethylacetate Complexes with Pyridine Bases as Ligands // Inorganic Chemistry. 1999. Vol. 38. No. 17. pp. 3764-3773.
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RIS
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TY - JOUR
DO - 10.1021/ic981292w
UR - https://doi.org/10.1021/ic981292w
TI - Bi- and Mononuclear Nickel(II) Trimethylacetate Complexes with Pyridine Bases as Ligands
T2 - Inorganic Chemistry
AU - Eremenko, Igor L.
AU - Nefedov, Sergei E
AU - Sidorov, Aleksei A.
AU - Golubnichaya, Margarita A
AU - Danilov, Pavel V.
AU - Ikorskii, Vladimir N
AU - Shvedenkov, Yury G.
AU - Novotortsev, Vladimir M.
AU - Moiseev, Ilya I
PY - 1999
DA - 1999/07/29
PB - American Chemical Society (ACS)
SP - 3764-3773
IS - 17
VL - 38
SN - 0020-1669
SN - 1520-510X
ER -
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@article{1999_Eremenko,
author = {Igor L. Eremenko and Sergei E Nefedov and Aleksei A. Sidorov and Margarita A Golubnichaya and Pavel V. Danilov and Vladimir N Ikorskii and Yury G. Shvedenkov and Vladimir M. Novotortsev and Ilya I Moiseev},
title = {Bi- and Mononuclear Nickel(II) Trimethylacetate Complexes with Pyridine Bases as Ligands},
journal = {Inorganic Chemistry},
year = {1999},
volume = {38},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/ic981292w},
number = {17},
pages = {3764--3773},
doi = {10.1021/ic981292w}
}
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Eremenko, Igor L., et al. “Bi- and Mononuclear Nickel(II) Trimethylacetate Complexes with Pyridine Bases as Ligands.” Inorganic Chemistry, vol. 38, no. 17, Jul. 1999, pp. 3764-3773. https://doi.org/10.1021/ic981292w.
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