New chelate complexes of copper and iron: Sythesis and impregnation into a polymer matrix from solution in supercritical carbon dioxide
E. Said-Galiyev
1
,
L Nikitin
1
,
R Vinokur
1
,
M. O. Gallyamov
1
,
M Kurykin
1
,
O. Petrova
1
,
B. V. Lokshin
1
,
I. Volkov
1
,
A. Khokhlov
1
,
K Schaumburg
1
Publication type: Journal Article
Publication date: 2000-11-15
scimago Q1
wos Q2
SJR: 0.828
CiteScore: 6.7
Impact factor: 3.9
ISSN: 08885885, 15205045
General Chemistry
General Chemical Engineering
Industrial and Manufacturing Engineering
Abstract
New chelate complexes of copper diiminate and iron diiminate were synthesized. Their physical characteristics have been studied. The diffusion of supercritical carbon dioxide (scCO2) into polyarylate (PAR) films and their impregnation with diiminates were investigated. The equilibrium degree of PAR swelling in scCO2 is about 10%. The conditions of impregnation (45 °C, 8 MPa, 1.5 h) were determined. The impregnation was confirmed by the FT-IR spectroscopic data. Thermal reduction of metal ions was investigated. Transformations of the chelate complexes on the polymer-film surface were studied by ESCA. The value of the Auger factor indicates that, after thermal reduction, the copper ion is in a nearly univalent state. The copper content in films is as large as 6.3 wt %; the iron content is 4.5 wt %. The FT-IR and ESCA spectroscopic studies showed that, in the course of impregnation, chelate complexes interact with functional groups of the polymer. Subsequent thermal reduction of metal in air results in diimi...
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GOST
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Said-Galiyev E. et al. New chelate complexes of copper and iron: Sythesis and impregnation into a polymer matrix from solution in supercritical carbon dioxide // Industrial & Engineering Chemistry Research. 2000. Vol. 39. No. 12. pp. 4891-4896.
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Said-Galiyev E., Nikitin L., Vinokur R., Gallyamov M. O., Kurykin M., Petrova O., Lokshin B. V., Volkov I., Khokhlov A., K Schaumburg New chelate complexes of copper and iron: Sythesis and impregnation into a polymer matrix from solution in supercritical carbon dioxide // Industrial & Engineering Chemistry Research. 2000. Vol. 39. No. 12. pp. 4891-4896.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/ie000251g
UR - https://doi.org/10.1021/ie000251g
TI - New chelate complexes of copper and iron: Sythesis and impregnation into a polymer matrix from solution in supercritical carbon dioxide
T2 - Industrial & Engineering Chemistry Research
AU - Said-Galiyev, E.
AU - Nikitin, L
AU - Vinokur, R
AU - Gallyamov, M. O.
AU - Kurykin, M
AU - Petrova, O.
AU - Lokshin, B. V.
AU - Volkov, I.
AU - Khokhlov, A.
AU - K Schaumburg
PY - 2000
DA - 2000/11/15
PB - American Chemical Society (ACS)
SP - 4891-4896
IS - 12
VL - 39
SN - 0888-5885
SN - 1520-5045
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2000_Said-Galiyev,
author = {E. Said-Galiyev and L Nikitin and R Vinokur and M. O. Gallyamov and M Kurykin and O. Petrova and B. V. Lokshin and I. Volkov and A. Khokhlov and K Schaumburg},
title = {New chelate complexes of copper and iron: Sythesis and impregnation into a polymer matrix from solution in supercritical carbon dioxide},
journal = {Industrial & Engineering Chemistry Research},
year = {2000},
volume = {39},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/ie000251g},
number = {12},
pages = {4891--4896},
doi = {10.1021/ie000251g}
}
Cite this
MLA
Copy
Said-Galiyev, E., et al. “New chelate complexes of copper and iron: Sythesis and impregnation into a polymer matrix from solution in supercritical carbon dioxide.” Industrial & Engineering Chemistry Research, vol. 39, no. 12, Nov. 2000, pp. 4891-4896. https://doi.org/10.1021/ie000251g.
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