Vanadia Gel Synthesis via Peroxovanadate Precursors. 1. In Situ Laser Raman and 51V NMR Characterization of the Gelation Process
Publication type: Journal Article
Publication date: 2000-11-17
scimago Q1
wos Q3
SJR: 0.742
CiteScore: 5.3
Impact factor: 2.9
ISSN: 15206106, 15205207, 10895647
Materials Chemistry
Surfaces, Coatings and Films
Physical and Theoretical Chemistry
Abstract
Vanadium oxide gels derived from aqueous solutions of V2O5 and H2O2 have been investigated using in situ 51V NMR and laser Raman spectroscopic techniques. On the basis of this characterization, a pathway for peroxovanadate decomposition has been proposed, including the presence of two peroxovanadate dimers. New Raman bands and assignments for these species are reported. Gelation was observed to begin both during and after the peroxovanadate decomposition, depending on the initial molar ratios of H2O2/V and the total concentration of vanadium. Experimental 51V NMR evidence suggested that the VO2+ species was directly involved in the formation of the gel.
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107
Total citations:
107
Citations from 2024:
3
(2.8%)
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Fontenot C. J. et al. Vanadia Gel Synthesis via Peroxovanadate Precursors. 1. In Situ Laser Raman and 51V NMR Characterization of the Gelation Process // Journal of Physical Chemistry B. 2000. Vol. 104. No. 49. pp. 11622-11631.
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Fontenot C. J., Wiench J. W., Pruski M., Schrader G. Vanadia Gel Synthesis via Peroxovanadate Precursors. 1. In Situ Laser Raman and 51V NMR Characterization of the Gelation Process // Journal of Physical Chemistry B. 2000. Vol. 104. No. 49. pp. 11622-11631.
Cite this
RIS
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TY - JOUR
DO - 10.1021/jp0021897
UR - https://doi.org/10.1021/jp0021897
TI - Vanadia Gel Synthesis via Peroxovanadate Precursors. 1. In Situ Laser Raman and 51V NMR Characterization of the Gelation Process
T2 - Journal of Physical Chemistry B
AU - Fontenot, Craig J
AU - Wiench, Jerzy W.
AU - Pruski, M.
AU - Schrader, G.L
PY - 2000
DA - 2000/11/17
PB - American Chemical Society (ACS)
SP - 11622-11631
IS - 49
VL - 104
SN - 1520-6106
SN - 1520-5207
SN - 1089-5647
ER -
Cite this
BibTex (up to 50 authors)
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@article{2000_Fontenot,
author = {Craig J Fontenot and Jerzy W. Wiench and M. Pruski and G.L Schrader},
title = {Vanadia Gel Synthesis via Peroxovanadate Precursors. 1. In Situ Laser Raman and 51V NMR Characterization of the Gelation Process},
journal = {Journal of Physical Chemistry B},
year = {2000},
volume = {104},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/jp0021897},
number = {49},
pages = {11622--11631},
doi = {10.1021/jp0021897}
}
Cite this
MLA
Copy
Fontenot, Craig J., et al. “Vanadia Gel Synthesis via Peroxovanadate Precursors. 1. In Situ Laser Raman and 51V NMR Characterization of the Gelation Process.” Journal of Physical Chemistry B, vol. 104, no. 49, Nov. 2000, pp. 11622-11631. https://doi.org/10.1021/jp0021897.