Organic Letters

, том 7 , издание 25 , страницы 5725-5727

Abnormally mild synthesis of bis(dithiolo)pyrroles from 2,5-dimethylpyrroles

Тип публикации: Journal Article

Дата публикации: 2005-11-17

American Chemical Society (ACS)

Organic Letters

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wos Q1

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SJR: 1.235

CiteScore: 8.7

Impact factor: 5.0

ISSN: 15237060, 15237052

DOI: 10.1021/ol052557v

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PubMed ID: 16321032

Organic Chemistry

Biochemistry

Physical and Theoretical Chemistry

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[chemical reaction: see text]. Treatment of N-substituted 2,5-dimethylpyrroles 2 with an equilibrated mixture of disulfur dichloride and DABCO in chloroform at 0 degrees C gives pentathiepinopyrroles 3 in moderate yields; further reaction of 3 with the same mixture at room temperature leads, in an extensive reaction cascade, to bis(dithiolo)pyrroles 4 in high yield; 2 can be converted into 4 in a one-pot operation under unusually mild conditions.

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Институт органической химии им. Н.Д. Зелинского РАН

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Amelichev S. A. et al. Abnormally mild synthesis of bis(dithiolo)pyrroles from 2,5-dimethylpyrroles // Organic Letters. 2005. Vol. 7. No. 25. pp. 5725-5727.

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Amelichev S. A., Aysin R., Aysin R. R., Konstantinova L. S., Obruchnikova N. V., Rakitin O. A., Rees C. W. Abnormally mild synthesis of bis(dithiolo)pyrroles from 2,5-dimethylpyrroles // Organic Letters. 2005. Vol. 7. No. 25. pp. 5725-5727.

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TY - JOUR

DO - 10.1021/ol052557v

UR - https://pubs.acs.org/doi/10.1021/ol052557v

TI - Abnormally mild synthesis of bis(dithiolo)pyrroles from 2,5-dimethylpyrroles

T2 - Organic Letters

AU - Amelichev, Stanislav A.

AU - Aysin, Rinat

AU - Aysin, Rinat R

AU - Konstantinova, Lidia S.

AU - Obruchnikova, Natalia V.

AU - Rakitin, Oleg A.

AU - Rees, Charles W.

PY - 2005

DA - 2005/11/17

PB - American Chemical Society (ACS)

SP - 5725-5727

IS - 25

VL - 7

PMID - 16321032

SN - 1523-7060

SN - 1523-7052

ER -

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@article{2005_Amelichev,

author = {Stanislav A. Amelichev and Rinat Aysin and Rinat R Aysin and Lidia S. Konstantinova and Natalia V. Obruchnikova and Oleg A. Rakitin and Charles W. Rees},

title = {Abnormally mild synthesis of bis(dithiolo)pyrroles from 2,5-dimethylpyrroles},

journal = {Organic Letters},

year = {2005},

volume = {7},

publisher = {American Chemical Society (ACS)},

month = {nov},

url = {https://pubs.acs.org/doi/10.1021/ol052557v},

number = {25},

pages = {5725--5727},

doi = {10.1021/ol052557v}

}

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Amelichev, Stanislav A., et al. “Abnormally mild synthesis of bis(dithiolo)pyrroles from 2,5-dimethylpyrroles.” Organic Letters, vol. 7, no. 25, Nov. 2005, pp. 5725-5727. https://pubs.acs.org/doi/10.1021/ol052557v.