Oxo/Imido Heterometathesis Reactions Catalyzed by a Silica-Supported Tantalum Imido Complex
Pavel A Zhizhko
1
,
Anton A Zhizhin
1
,
Olga A Belyakova
1
,
Yan V. Zubavichus
1, 2
,
Yuriy G Kolyagin
3
,
Dmitry N. Zarubin
1
,
N. A. Ustynyuk
1
Publication type: Journal Article
Publication date: 2013-06-25
scimago Q2
wos Q1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Grafting Ta(═NtBu)(CH2CMe2Ph)3 onto the surface of silica partially dehydroxylated at 300 °C leads to the formation of the surface imido complex (≡SiO)2Ta(═NtBu)(CH2CMe2Ph) as a major species, which was characterized with EXAFS, 13C CP/MAS NMR, diffuse reflectance FTIR, elemental analyses, and chemical reactivity. The obtained material acts as an efficient heterogeneous catalyst for various oxo/imido heterometathesis transformations: imidation of ketones and DMF with N-sulfinylamines and condensation of N-sulfinylamines into sulfurdiimines and phenyl isocyanate into diphenylcarbodiimide.
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Total citations:
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GOST
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Zhizhko P. A. et al. Oxo/Imido Heterometathesis Reactions Catalyzed by a Silica-Supported Tantalum Imido Complex // Organometallics. 2013. Vol. 32. No. 13. pp. 3611-3617.
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Zhizhko P. A., Zhizhin A. A., Belyakova O. A., Zubavichus Y. V., Kolyagin Y. G., Zarubin D. N., Ustynyuk N. A. Oxo/Imido Heterometathesis Reactions Catalyzed by a Silica-Supported Tantalum Imido Complex // Organometallics. 2013. Vol. 32. No. 13. pp. 3611-3617.
Cite this
RIS
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TY - JOUR
DO - 10.1021/om4001499
UR - https://doi.org/10.1021/om4001499
TI - Oxo/Imido Heterometathesis Reactions Catalyzed by a Silica-Supported Tantalum Imido Complex
T2 - Organometallics
AU - Zhizhko, Pavel A
AU - Zhizhin, Anton A
AU - Belyakova, Olga A
AU - Zubavichus, Yan V.
AU - Kolyagin, Yuriy G
AU - Zarubin, Dmitry N.
AU - Ustynyuk, N. A.
PY - 2013
DA - 2013/06/25
PB - American Chemical Society (ACS)
SP - 3611-3617
IS - 13
VL - 32
SN - 0276-7333
SN - 1520-6041
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2013_Zhizhko,
author = {Pavel A Zhizhko and Anton A Zhizhin and Olga A Belyakova and Yan V. Zubavichus and Yuriy G Kolyagin and Dmitry N. Zarubin and N. A. Ustynyuk},
title = {Oxo/Imido Heterometathesis Reactions Catalyzed by a Silica-Supported Tantalum Imido Complex},
journal = {Organometallics},
year = {2013},
volume = {32},
publisher = {American Chemical Society (ACS)},
month = {jun},
url = {https://doi.org/10.1021/om4001499},
number = {13},
pages = {3611--3617},
doi = {10.1021/om4001499}
}
Cite this
MLA
Copy
Zhizhko, Pavel A., et al. “Oxo/Imido Heterometathesis Reactions Catalyzed by a Silica-Supported Tantalum Imido Complex.” Organometallics, vol. 32, no. 13, Jun. 2013, pp. 3611-3617. https://doi.org/10.1021/om4001499.