Open Access

Nature Communications, volume 10, issue 1, publication number 2994

High-pressure synthesis of ultraincompressible hard rhenium nitride pernitride Re2(N2)(N)2 stable at ambient conditions

Maxim Bykov ¹

Stella Chariton ¹

Hongzhan Fei ¹

Timofey Fedotenko ²

Georgios Aprilis ²

Alena V Ponomareva ³

Ferenc Tasnádi ⁴

Igor A Abrikosov ⁴

Benoit Merle ⁵

Patrick Feldner ⁵

SEBASTIAN VOGEL ⁶

Wolfgang Schnick ⁶

Vitali B. Prakapenka ⁷

E. Greenberg ⁷

Michael Hanfland ⁸

Anna Pakhomova ⁹

H.-P. Liermann ⁹

Tomoo Katsura ¹

N.A. Dubrovinskaia ²

L. Dubrovinsky ¹

Hide authors affiliations Show authors affiliations: 9 affiliations

Bayerisches GeoInstitut, University of Bayreuth, Bayreuth, Germany |

Material Physics and Technology at Extreme Conditions, Laboratory of Crystallography, University of Bayreuth, Bayreuth, Germany |

Materials Modeling and Development Laboratory, National University of Science and Technology ‘MISIS’, Moscow, Russia |

⁴

Department of Physics, Chemistry and Biology (IFM), Linköping University, Linköping, Sweden |

⁵

Materials Science and Engineering, Institute I, Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU) Martensstraβe. 5, Erlangen, Germany |

⁶

Chair in Inorganic Solid State Chemistry, Department of Chemistry, University of Munich (LMU), Munich, Germany |

⁷

Center for Advanced Radiation Sources, University of Chicago, Chicago, USA |

⁸

European Synchrotron Radiation Facility, Grenoble cedex, France |

⁹

Photon Science, Deutsches Elektronen-Synchrotron, Hamburg, Germany |

Publication type: Journal Article

Publication date: 2019-07-05

Springer Nature

Journal: Nature Communications

Quartile SCImago

Quartile WOS

Impact factor: 16.6

ISSN: 20411723, 20411723

DOI: 10.1038/s41467-019-10995-3

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PubMed ID: 31278267

General Chemistry

General Biochemistry, Genetics and Molecular Biology

Multidisciplinary

General Physics and Astronomy

Abstract

High-pressure synthesis in diamond anvil cells can yield unique compounds with advanced properties, but often they are either unrecoverable at ambient conditions or produced in quantity insufficient for properties characterization. Here we report the synthesis of metallic, ultraincompressible (K0 = 428(10) GPa), and very hard (nanoindentation hardness 36.7(8) GPa) rhenium nitride pernitride Re2(N2)(N)2. Unlike known transition metals pernitrides Re2(N2)(N)2 contains both pernitride N24− and discrete N3− anions, which explains its exceptional properties. Re2(N2)(N)2 can be obtained via a reaction between rhenium and nitrogen in a diamond anvil cell at pressures from 40 to 90 GPa and is recoverable at ambient conditions. We develop a route to scale up its synthesis through a reaction between rhenium and ammonium azide, NH4N3, in a large-volume press at 33 GPa. Although metallic bonding is typically seen incompatible with intrinsic hardness, Re2(N2)(N)2 turned to be at a threshold for superhard materials. High pressure experiments may yield materials with unusual combinations of properties, but typically in small amounts and unstable. Here the authors synthesize millimeter-sized samples of metallic, ultraincompressible and very hard rhenium nitride pernitride, recoverable at ambient conditions.

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Citations by journals

	1 2 3 4
Inorganic Chemistry	Inorganic Chemistry, 4, 5.63% Inorganic Chemistry 4 publications, 5.63%
Review of Scientific Instruments	Review of Scientific Instruments, 3, 4.23% Review of Scientific Instruments 3 publications, 4.23%
Angewandte Chemie	Angewandte Chemie, 3, 4.23% Angewandte Chemie 3 publications, 4.23%
Angewandte Chemie - International Edition	Angewandte Chemie - International Edition, 3, 4.23% Angewandte Chemie - International Edition 3 publications, 4.23%
Physical Chemistry Chemical Physics	Physical Chemistry Chemical Physics, 3, 4.23% Physical Chemistry Chemical Physics 3 publications, 4.23%
Physical Review Materials	Physical Review Materials, 2, 2.82% Physical Review Materials 2 publications, 2.82%
Physical Review B	Physical Review B, 2, 2.82% Physical Review B 2 publications, 2.82%
Coordination Chemistry Reviews	Coordination Chemistry Reviews, 2, 2.82% Coordination Chemistry Reviews 2 publications, 2.82%
European Journal of Inorganic Chemistry	European Journal of Inorganic Chemistry, 2, 2.82% European Journal of Inorganic Chemistry 2 publications, 2.82%
Journal of Physical Chemistry C	Journal of Physical Chemistry C, 2, 2.82% Journal of Physical Chemistry C 2 publications, 2.82%
ACS Nano	ACS Nano, 2, 2.82% ACS Nano 2 publications, 2.82%
Dalton Transactions	Dalton Transactions, 2, 2.82% Dalton Transactions 2 publications, 2.82%
Journal of Materials Chemistry A	Journal of Materials Chemistry A, 2, 2.82% Journal of Materials Chemistry A 2 publications, 2.82%
Nature Communications	Nature Communications, 2, 2.82% Nature Communications 2 publications, 2.82%
Physical Review Letters	Physical Review Letters, 1, 1.41% Physical Review Letters 1 publication, 1.41%
Journal of Applied Physics	Journal of Applied Physics, 1, 1.41% Journal of Applied Physics 1 publication, 1.41%
Journal of Chemical Physics	Journal of Chemical Physics, 1, 1.41% Journal of Chemical Physics 1 publication, 1.41%
Applied Physics Letters	Applied Physics Letters, 1, 1.41% Applied Physics Letters 1 publication, 1.41%
AIP Advances	AIP Advances, 1, 1.41% AIP Advances 1 publication, 1.41%
Journal of Synchrotron Radiation	Journal of Synchrotron Radiation, 1, 1.41% Journal of Synchrotron Radiation 1 publication, 1.41%
Crystals	Crystals, 1, 1.41% Crystals 1 publication, 1.41%
Nature	Nature, 1, 1.41% Nature 1 publication, 1.41%
Nature Reviews Chemistry	Nature Reviews Chemistry, 1, 1.41% Nature Reviews Chemistry 1 publication, 1.41%
Journal of Alloys and Compounds	Journal of Alloys and Compounds, 1, 1.41% Journal of Alloys and Compounds 1 publication, 1.41%
Surface and Coatings Technology	Surface and Coatings Technology, 1, 1.41% Surface and Coatings Technology 1 publication, 1.41%
Journal of Energy Chemistry	Journal of Energy Chemistry, 1, 1.41% Journal of Energy Chemistry 1 publication, 1.41%
Journal of Physics: Conference Series	Journal of Physics: Conference Series, 1, 1.41% Journal of Physics: Conference Series 1 publication, 1.41%
Applied Physics Express	Applied Physics Express, 1, 1.41% Applied Physics Express 1 publication, 1.41%
Chemical Physics	Chemical Physics, 1, 1.41% Chemical Physics 1 publication, 1.41%
	1 2 3 4

Citations by publishers

	2 4 6 8 10 12 14 16
Wiley	Wiley, 16, 22.54% Wiley 16 publications, 22.54%
American Chemical Society (ACS)	American Chemical Society (ACS), 11, 15.49% American Chemical Society (ACS) 11 publications, 15.49%
Elsevier	Elsevier, 10, 14.08% Elsevier 10 publications, 14.08%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 10, 14.08% Royal Society of Chemistry (RSC) 10 publications, 14.08%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 8, 11.27% American Institute of Physics (AIP) 8 publications, 11.27%
American Physical Society (APS)	American Physical Society (APS), 5, 7.04% American Physical Society (APS) 5 publications, 7.04%
Springer Nature	Springer Nature, 4, 5.63% Springer Nature 4 publications, 5.63%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 1, 1.41% Multidisciplinary Digital Publishing Institute (MDPI) 1 publication, 1.41%
IOP Publishing	IOP Publishing, 1, 1.41% IOP Publishing 1 publication, 1.41%
Japan Society of Applied Physics	Japan Society of Applied Physics, 1, 1.41% Japan Society of Applied Physics 1 publication, 1.41%
International Union of Crystallography (IUCr)	International Union of Crystallography (IUCr), 1, 1.41% International Union of Crystallography (IUCr) 1 publication, 1.41%
OAE Publishing Inc.	OAE Publishing Inc., 1, 1.41% OAE Publishing Inc. 1 publication, 1.41%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 1.41% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 1.41%
	2 4 6 8 10 12 14 16

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Bykov M. et al. High-pressure synthesis of ultraincompressible hard rhenium nitride pernitride Re2(N2)(N)2 stable at ambient conditions // Nature Communications. 2019. Vol. 10. No. 1. 2994

GOST all authors (up to 50) Copy

Bykov M., Chariton S., Fei H., Fedotenko T., Aprilis G., Ponomareva A. V., Tasnádi F., Abrikosov I. A., Merle B., Feldner P., VOGEL S., Schnick W., Prakapenka V. B., Greenberg E., Hanfland M., Pakhomova A., Liermann H., Katsura T., Dubrovinskaia N., Dubrovinsky L. High-pressure synthesis of ultraincompressible hard rhenium nitride pernitride Re2(N2)(N)2 stable at ambient conditions // Nature Communications. 2019. Vol. 10. No. 1. 2994

RIS |

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TY - JOUR

DO - 10.1038/s41467-019-10995-3

UR - https://doi.org/10.1038/s41467-019-10995-3

TI - High-pressure synthesis of ultraincompressible hard rhenium nitride pernitride Re2(N2)(N)2 stable at ambient conditions

T2 - Nature Communications

AU - Bykov, Maxim

AU - Chariton, Stella

AU - Fei, Hongzhan

AU - Fedotenko, Timofey

AU - Aprilis, Georgios

AU - Ponomareva, Alena V

AU - Tasnádi, Ferenc

AU - Abrikosov, Igor A

AU - Merle, Benoit

AU - Feldner, Patrick

AU - VOGEL, SEBASTIAN

AU - Schnick, Wolfgang

AU - Prakapenka, Vitali B.

AU - Greenberg, E.

AU - Hanfland, Michael

AU - Pakhomova, Anna

AU - Liermann, H.-P.

AU - Katsura, Tomoo

AU - Dubrovinskaia, N.A.

AU - Dubrovinsky, L.

PY - 2019

DA - 2019/07/05 00:00:00

PB - Springer Nature

IS - 1

VL - 10

PMID - 31278267

SN - 2041-1723

ER -

BibTex

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BibTex Copy

@article{2019_Bykov,

author = {Maxim Bykov and Stella Chariton and Hongzhan Fei and Timofey Fedotenko and Georgios Aprilis and Alena V Ponomareva and Ferenc Tasnádi and Igor A Abrikosov and Benoit Merle and Patrick Feldner and SEBASTIAN VOGEL and Wolfgang Schnick and Vitali B. Prakapenka and E. Greenberg and Michael Hanfland and Anna Pakhomova and H.-P. Liermann and Tomoo Katsura and N.A. Dubrovinskaia and L. Dubrovinsky},

title = {High-pressure synthesis of ultraincompressible hard rhenium nitride pernitride Re2(N2)(N)2 stable at ambient conditions},

journal = {Nature Communications},

year = {2019},

volume = {10},

publisher = {Springer Nature},

month = {jul},

url = {https://doi.org/10.1038/s41467-019-10995-3},

number = {1},

doi = {10.1038/s41467-019-10995-3}

}

Found error?

Publisher

Springer Nature

Journal

Nature Communications

Quartile SCImago

Quartile WOS

Impact factor

16.6

ISSN

20411723 (Print)
20411723 (Electronic)