Siloxane-containing derivatives of benzoic acid: chemical transformation of the carboxyl group
3
HZ University of Applied Sciences, 4382 NW Middelburg, The Netherlands
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Publication type: Journal Article
Publication date: 2022-09-02
scimago Q2
wos Q3
SJR: 0.493
CiteScore: 5.0
Impact factor: 2.5
ISSN: 11440546, 13699261
Materials Chemistry
General Chemistry
Catalysis
Abstract
This study presents a route for chemical transformation of Si-derivatives of benzoic acid – p-carboxyphenyldisiloxane and bis(p-carboxyphenyl)disiloxane – to a wide range of corresponding esters, thioesters, amides, etc. The reactions proceed under mild reaction conditions, in the presence of carbonyldiimidazole as a carboxyl group activator, making it possible to obtain the desired products in gram scale with high selectivity (without destruction of the organosiloxane backbone) and yields up to 97%. The structure of the resulting compounds was confirmed by IR, HRMS ESI, 1D and 2D 1H/13C/29Si NMR spectroscopy, and X-ray diffraction data. It is shown by the example of some Si-derivatives of amides, that they form HOF-like structures in the crystalline state.
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Goncharova I. K. et al. Siloxane-containing derivatives of benzoic acid: chemical transformation of the carboxyl group // New Journal of Chemistry. 2022. Vol. 46. No. 37. pp. 18041-18047.
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Goncharova I. K., Ulianova E. A., Novikov R. G., Volodin A. D., Korlyukov A., Arzumanyan A. V. Siloxane-containing derivatives of benzoic acid: chemical transformation of the carboxyl group // New Journal of Chemistry. 2022. Vol. 46. No. 37. pp. 18041-18047.
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RIS
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TY - JOUR
DO - 10.1039/d2nj03872b
UR - https://xlink.rsc.org/?DOI=D2NJ03872B
TI - Siloxane-containing derivatives of benzoic acid: chemical transformation of the carboxyl group
T2 - New Journal of Chemistry
AU - Goncharova, Irina K
AU - Ulianova, Eva A
AU - Novikov, Roman G.
AU - Volodin, Alexander D
AU - Korlyukov, Alexander
AU - Arzumanyan, Ashot V
PY - 2022
DA - 2022/09/02
PB - Royal Society of Chemistry (RSC)
SP - 18041-18047
IS - 37
VL - 46
SN - 1144-0546
SN - 1369-9261
ER -
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BibTex (up to 50 authors)
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@article{2022_Goncharova,
author = {Irina K Goncharova and Eva A Ulianova and Roman G. Novikov and Alexander D Volodin and Alexander Korlyukov and Ashot V Arzumanyan},
title = {Siloxane-containing derivatives of benzoic acid: chemical transformation of the carboxyl group},
journal = {New Journal of Chemistry},
year = {2022},
volume = {46},
publisher = {Royal Society of Chemistry (RSC)},
month = {sep},
url = {https://xlink.rsc.org/?DOI=D2NJ03872B},
number = {37},
pages = {18041--18047},
doi = {10.1039/d2nj03872b}
}
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MLA
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Goncharova, Irina K., et al. “Siloxane-containing derivatives of benzoic acid: chemical transformation of the carboxyl group.” New Journal of Chemistry, vol. 46, no. 37, Sep. 2022, pp. 18041-18047. https://xlink.rsc.org/?DOI=D2NJ03872B.