Copper(i) halide and palladium(ii) chloride complexes of 4-thioxo[1,3,5]oxadiazocines: Synthesis, structure and antibacterial activity
Andrey S. Kuzovlev
1, 2, 3, 4, 5
,
Daria A Volkova
1, 2, 3, 4, 5
,
Irina V Parfenova
1, 2, 3, 4, 5
,
Ivan V. Kulakov
1, 2, 3, 4, 5
,
Alena O Shkirdova
5, 6, 7, 8, 9
,
V. V. Chernyshev
5, 6, 7, 8, 9, 10, 11
,
Victor B. Rybakov
5, 10, 11, 12, 13
,
Nikolay N Fefilov
1, 2, 3, 4, 5
,
Alexey S. Vasilchenko
3, 4, 5, 14, 15, 16
2
Institute of Chemistry
4
625003 Tyumen
|
5
RUSSIAN FEDERATION
|
7
Laboratory of New Physicochemical Problems
9
119071 Moscow
11
DEPARTMENT OF CHEMISTRY
13
119991 Moscow
15
Laboratory of Antimicrobial Resistance
16
Institute of Environmental and Agricultural Biology (X-BIO)
Publication type: Journal Article
Publication date: 2020-04-13
scimago Q2
wos Q3
SJR: 0.493
CiteScore: 5.0
Impact factor: 2.5
ISSN: 11440546, 13699261
Materials Chemistry
General Chemistry
Catalysis
Abstract
Copper(I) halide and palladium(II) chloride complexes with tricyclic monastrol analogs containing the oxadiazocine ring have been synthesized and studied. The structures of the complexes were investigated with IR, NMR and UV spectroscopy. Two complexes, [Cu(L1)2Cl] and [Pd(L1)2Cl2], were structurally characterized by X-ray single-crystal and powder diffraction respectively. All the obtained coordination compounds were mononuclear. The ligands were coordinated with copper(I) and palladium(II) only via the soft sulfur atoms of thiocarbamide fragments, while the harder nitrogen and oxygen atoms remained uncoordinated. The palladium center was coordinated by two Cl ions and two S atoms from two 4-thioxo[1,3,5]oxadiazocine ligands in a distorted square-planar geometry. Copper(I) formed a trigonal planar geometry. The complexes demonstrated significant antibacterial activity towards the Escherichia coli K12 TG 1 bacterial strain in contrast to the free ligands, which didn’t show any noticeable activity.
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Kuzovlev A. S. et al. Copper(i) halide and palladium(ii) chloride complexes of 4-thioxo[1,3,5]oxadiazocines: Synthesis, structure and antibacterial activity // New Journal of Chemistry. 2020. Vol. 44. No. 19. pp. 7865-7875.
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Kuzovlev A. S., Volkova D. A., Parfenova I. V., Kulakov I. V., Shkirdova A. O., Zamilatskov I. A., Chernyshev V. V., Rybakov V. B., Tyurin V. S., Fefilov N. N., Vasilchenko A. S. Copper(i) halide and palladium(ii) chloride complexes of 4-thioxo[1,3,5]oxadiazocines: Synthesis, structure and antibacterial activity // New Journal of Chemistry. 2020. Vol. 44. No. 19. pp. 7865-7875.
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TY - JOUR
DO - 10.1039/c9nj05958j
UR - https://xlink.rsc.org/?DOI=C9NJ05958J
TI - Copper(i) halide and palladium(ii) chloride complexes of 4-thioxo[1,3,5]oxadiazocines: Synthesis, structure and antibacterial activity
T2 - New Journal of Chemistry
AU - Kuzovlev, Andrey S.
AU - Volkova, Daria A
AU - Parfenova, Irina V
AU - Kulakov, Ivan V.
AU - Shkirdova, Alena O
AU - Zamilatskov, Ilya A.
AU - Chernyshev, V. V.
AU - Rybakov, Victor B.
AU - Tyurin, Vladimir S
AU - Fefilov, Nikolay N
AU - Vasilchenko, Alexey S.
PY - 2020
DA - 2020/04/13
PB - Royal Society of Chemistry (RSC)
SP - 7865-7875
IS - 19
VL - 44
SN - 1144-0546
SN - 1369-9261
ER -
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@article{2020_Kuzovlev,
author = {Andrey S. Kuzovlev and Daria A Volkova and Irina V Parfenova and Ivan V. Kulakov and Alena O Shkirdova and Ilya A. Zamilatskov and V. V. Chernyshev and Victor B. Rybakov and Vladimir S Tyurin and Nikolay N Fefilov and Alexey S. Vasilchenko},
title = {Copper(i) halide and palladium(ii) chloride complexes of 4-thioxo[1,3,5]oxadiazocines: Synthesis, structure and antibacterial activity},
journal = {New Journal of Chemistry},
year = {2020},
volume = {44},
publisher = {Royal Society of Chemistry (RSC)},
month = {apr},
url = {https://xlink.rsc.org/?DOI=C9NJ05958J},
number = {19},
pages = {7865--7875},
doi = {10.1039/c9nj05958j}
}
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MLA
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Kuzovlev, Andrey S., et al. “Copper(i) halide and palladium(ii) chloride complexes of 4-thioxo[1,3,5]oxadiazocines: Synthesis, structure and antibacterial activity.” New Journal of Chemistry, vol. 44, no. 19, Apr. 2020, pp. 7865-7875. https://xlink.rsc.org/?DOI=C9NJ05958J.