Open Access
Acta Crystallographica Section E: Crystallographic Communications, volume 74, issue 10, pages 1392-1395
Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain
Maxim Bykov
1
,
Saiana Khandarkhaeva
1
,
Timofey Fedotenko
2
,
Pavel Sedmak
3
,
Natalia Dubrovinskaia
2
,
Leonid Dubrovinsky
1
Publication type: Journal Article
Publication date: 2018-09-07
Quartile SCImago
Q3
Quartile WOS
—
Impact factor: 0.6
ISSN: 20569890
PubMed ID:
30319786
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
Iron tetranitride, FeN4, was synthesized from the elements in a laser-heated diamond anvil cell at 180 (5) GPa and 2700 (200) K. Its crystal structure was determined based on single-crystal X-ray diffraction data collected from a submicron-sized grain at the synchrotron beamline ID11 of ESRF. The compound crystallizes in the triclinic space groupP\overline{1}. In the asymmetric unit, the Fe atom occupies an inversion centre (Wyckoff position 1d), while two N atoms occupy general positions (2i). The structure is made up from edge-sharing [FeN6] octahedra forming chains along [100] and being interconnected through N—N bridges. N atoms formcatena-poly[tetraz-1-ene-1,4-diyl] anions [–N=N—N—N–]∞2−running along [001]. In comparison with the previously reported structure of FeN4at 135 GPa [Bykovet al.(2018).Nat. Commun.9, 2756], the crystal structure of FeN4at 180 GPa is similar but the structural model is significantly improved in terms of the precision of the bond lengths and angles.
Top-30
Citations by journals
|
1
2
|
|
|
Journal of Alloys and Compounds
2 publications, 6.67%
|
|
|
European Journal of Inorganic Chemistry
2 publications, 6.67%
|
|
|
Angewandte Chemie - International Edition
2 publications, 6.67%
|
|
|
Angewandte Chemie
2 publications, 6.67%
|
|
|
Inorganic Chemistry
2 publications, 6.67%
|
|
|
Journal of Physical Chemistry C
2 publications, 6.67%
|
|
|
Journal of Physical Chemistry Letters
2 publications, 6.67%
|
|
|
Physical Review Letters
1 publication, 3.33%
|
|
|
Review of Scientific Instruments
1 publication, 3.33%
|
|
|
Materials
1 publication, 3.33%
|
|
|
Nature
1 publication, 3.33%
|
|
|
Nature Communications
1 publication, 3.33%
|
|
|
Journal of Physics Condensed Matter
1 publication, 3.33%
|
|
|
Applied Physics Express
1 publication, 3.33%
|
|
|
Physics Letters, Section A: General, Atomic and Solid State Physics
1 publication, 3.33%
|
|
|
Current Opinion in Solid State and Materials Science
1 publication, 3.33%
|
|
|
Nanoscale
1 publication, 3.33%
|
|
|
Physical Chemistry Chemical Physics
1 publication, 3.33%
|
|
|
Physical Review B
1 publication, 3.33%
|
|
|
Russian Chemical Reviews
1 publication, 3.33%
|
|
|
Chinese Physics Letters
1 publication, 3.33%
|
|
|
Journal of the American Chemical Society
1 publication, 3.33%
|
|
|
Chemistry of Materials
1 publication, 3.33%
|
|
|
1
2
|
Citations by publishers
|
1
2
3
4
5
6
7
8
|
|
|
American Chemical Society (ACS)
8 publications, 26.67%
|
|
|
Wiley
6 publications, 20%
|
|
|
Elsevier
4 publications, 13.33%
|
|
|
American Physical Society (APS)
2 publications, 6.67%
|
|
|
Springer Nature
2 publications, 6.67%
|
|
|
IOP Publishing
2 publications, 6.67%
|
|
|
Royal Society of Chemistry (RSC)
2 publications, 6.67%
|
|
|
American Institute of Physics (AIP)
1 publication, 3.33%
|
|
|
Multidisciplinary Digital Publishing Institute (MDPI)
1 publication, 3.33%
|
|
|
Japan Society of Applied Physics
1 publication, 3.33%
|
|
|
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii
1 publication, 3.33%
|
|
|
1
2
3
4
5
6
7
8
|
- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
{"yearsCitations":{"type":"bar","data":{"show":true,"labels":[2019,2020,2021,2022,2023,2024],"ids":[0,0,0,0,0,0],"codes":[0,0,0,0,0,0],"imageUrls":["","","","","",""],"datasets":[{"label":"Citations number","data":[6,7,6,3,2,6],"backgroundColor":["#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6"],"percentage":["20","23.33","20","10","6.67","20"],"barThickness":null}]},"options":{"indexAxis":"x","maintainAspectRatio":true,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":false},"x":{"ticks":{"stepSize":1,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":false}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Citations per year","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}},"journals":{"type":"bar","data":{"show":true,"labels":["Journal of Alloys and Compounds","European Journal of Inorganic Chemistry","Angewandte Chemie - International Edition","Angewandte Chemie","Inorganic Chemistry","Journal of Physical Chemistry C","Journal of Physical Chemistry Letters","Physical Review Letters","Review of Scientific Instruments","Materials","Nature","Nature Communications","Journal of Physics Condensed Matter","Applied Physics Express","Physics Letters, Section A: General, Atomic and Solid State Physics","Current Opinion in Solid State and Materials Science","Nanoscale","Physical Chemistry Chemical Physics","Physical Review B","Russian Chemical Reviews","Chinese Physics Letters","Journal of the American Chemical Society","Chemistry of Materials"],"ids":[4015,15359,19215,25450,24714,8859,21963,4343,10899,25198,14611,3231,4579,24517,2947,24572,228,1773,25280,23802,22690,4813,6428],"codes":[0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0,0],"imageUrls":["\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/bRyGpdm98BkAUYiK1YFNpl5Z7hPu6Gd87gbIeuG3_medium.webp","\/storage\/images\/resized\/bRyGpdm98BkAUYiK1YFNpl5Z7hPu6Gd87gbIeuG3_medium.webp","\/storage\/images\/resized\/bRyGpdm98BkAUYiK1YFNpl5Z7hPu6Gd87gbIeuG3_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/nrK64iXHTzj43wMrfN1ZoUQ0vanswGzWPN45K3jA_medium.webp","\/storage\/images\/resized\/ARM4e6URKRsbRZvIF0vFis9DjxGloBjnBYJXbHmZ_medium.webp","\/storage\/images\/resized\/MjH1ITP7lMYGxeqUZfkt2BnVLgjkk413jwBV97XX_medium.webp","\/storage\/images\/resized\/voXLqlsvTwv5p3iMQ8Dhs95nqB4AXOG7Taj7G4ra_medium.webp","\/storage\/images\/resized\/voXLqlsvTwv5p3iMQ8Dhs95nqB4AXOG7Taj7G4ra_medium.webp","\/storage\/images\/resized\/LsKy6OnmmmRGcAU6CZgWQvNiP1polbaSLNrN7zqj_medium.webp","\/storage\/images\/resized\/wFULTOy1QTD7DkRFxasdNYr8tnVZXl2nkWAWWTzz_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/leiAYcRDGTSl5B1eCnwpSGqmDEUEfDPPoYisFGhT_medium.webp","\/storage\/images\/resized\/leiAYcRDGTSl5B1eCnwpSGqmDEUEfDPPoYisFGhT_medium.webp","\/storage\/images\/resized\/nrK64iXHTzj43wMrfN1ZoUQ0vanswGzWPN45K3jA_medium.webp","\/storage\/images\/resized\/9Mus3KG1Tkd7Bwaurt8H3RwWh0CxRlGoO6ng9UK1_medium.webp","\/storage\/images\/resized\/LsKy6OnmmmRGcAU6CZgWQvNiP1polbaSLNrN7zqj_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp"],"datasets":[{"label":"","data":[2,2,2,2,2,2,2,1,1,1,1,1,1,1,1,1,1,1,1,1,1,1,1],"backgroundColor":["#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6"],"percentage":[6.67,6.67,6.67,6.67,6.67,6.67,6.67,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33,3.33],"barThickness":13}]},"options":{"indexAxis":"y","maintainAspectRatio":false,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":false},"x":{"ticks":{"stepSize":null,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":false}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Journals","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}},"publishers":{"type":"bar","data":{"show":true,"labels":["American Chemical Society (ACS)","Wiley","Elsevier","American Physical Society (APS)","Springer Nature","IOP Publishing","Royal Society of Chemistry (RSC)","American Institute of Physics (AIP)","Multidisciplinary Digital Publishing Institute (MDPI)","Japan Society of Applied Physics","Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii"],"ids":[40,11,17,1539,8,2075,123,250,202,804,9422],"codes":[0,0,0,0,0,0,0,0,0,0,0],"imageUrls":["\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/bRyGpdm98BkAUYiK1YFNpl5Z7hPu6Gd87gbIeuG3_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/nrK64iXHTzj43wMrfN1ZoUQ0vanswGzWPN45K3jA_medium.webp","\/storage\/images\/resized\/voXLqlsvTwv5p3iMQ8Dhs95nqB4AXOG7Taj7G4ra_medium.webp","\/storage\/images\/resized\/LsKy6OnmmmRGcAU6CZgWQvNiP1polbaSLNrN7zqj_medium.webp","\/storage\/images\/resized\/leiAYcRDGTSl5B1eCnwpSGqmDEUEfDPPoYisFGhT_medium.webp","\/storage\/images\/resized\/ARM4e6URKRsbRZvIF0vFis9DjxGloBjnBYJXbHmZ_medium.webp","\/storage\/images\/resized\/MjH1ITP7lMYGxeqUZfkt2BnVLgjkk413jwBV97XX_medium.webp","\/storage\/images\/resized\/wFULTOy1QTD7DkRFxasdNYr8tnVZXl2nkWAWWTzz_medium.webp","\/storage\/images\/resized\/9Mus3KG1Tkd7Bwaurt8H3RwWh0CxRlGoO6ng9UK1_medium.webp"],"datasets":[{"label":"","data":[8,6,4,2,2,2,2,1,1,1,1],"backgroundColor":["#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6"],"percentage":[26.67,20,13.33,6.67,6.67,6.67,6.67,3.33,3.33,3.33,3.33],"barThickness":13}]},"options":{"indexAxis":"y","maintainAspectRatio":false,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":false},"x":{"ticks":{"stepSize":null,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":false}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Publishers","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}},"yearsCitationsQuartiles":{"type":"bar","data":{"show":true,"labels":[2019,2020,2021,2022,2023,2024],"ids":[],"codes":[],"imageUrls":[],"datasets":[{"label":"Q4","backgroundColor":"rgb(221,90,78)","data":[0,0,0,0,0,0],"percentage":["0","0","0","0","0","0"]},{"label":"Q3","backgroundColor":"rgb(251, 163,83)","data":[0,0,0,0,0,0],"percentage":["0","0","0","0","0","0"]},{"label":"Q2","backgroundColor":"rgb(232, 213, 89)","data":[3,1,2,1,0,0],"percentage":["10","3.33","6.67","3.33","0","0"]},{"label":"Q1","backgroundColor":"rgb(164, 207, 99)","data":[3,6,4,2,2,6],"percentage":["10","20","13.33","6.67","6.67","20"]},{"label":"Quartile not defined","backgroundColor":"#E5E7EB","data":[0,0,0,0,0,0],"percentage":["0","0","0","0","0","0"]}]},"options":{"indexAxis":"x","maintainAspectRatio":true,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":true},"x":{"ticks":{"stepSize":1,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":true}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Citations quartiles by SCImago per year","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}},"yearsCitationsQuartilesWs":{"type":"bar","data":{"show":true,"labels":[2019,2020,2021,2022,2023,2024],"ids":[],"codes":[],"imageUrls":[],"datasets":[{"label":"Q4","backgroundColor":"rgb(221,90,78)","data":[0,0,0,0,0,0],"percentage":["0","0","0","0","0","0"]},{"label":"Q3","backgroundColor":"rgb(251, 163,83)","data":[2,0,1,1,0,0],"percentage":["6.67","0","3.33","3.33","0","0"]},{"label":"Q2","backgroundColor":"rgb(232, 213, 89)","data":[1,3,1,0,1,2],"percentage":["3.33","10","3.33","0","3.33","6.67"]},{"label":"Q1","backgroundColor":"rgb(164, 207, 99)","data":[3,3,3,2,1,4],"percentage":["10","10","10","6.67","3.33","13.33"]},{"label":"Quartile not defined","backgroundColor":"#E5E7EB","data":[0,1,1,0,0,0],"percentage":["0","3.33","3.33","0","0","0"]}]},"options":{"indexAxis":"x","maintainAspectRatio":true,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":true},"x":{"ticks":{"stepSize":1,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"},"stacked":true}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Citations quartiles by WoS per year","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}}}
Are you a researcher?
Create a profile to get free access to personal recommendations for colleagues and new articles.
Metrics
Cite this
GOST |
RIS |
BibTex |
MLA
Cite this
GOST
Copy
Bykov M. et al. Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain // Acta Crystallographica Section E: Crystallographic Communications. 2018. Vol. 74. No. 10. pp. 1392-1395.
GOST all authors (up to 50)
Copy
Bykov M., Khandarkhaeva S., Fedotenko T., Sedmak P., Dubrovinskaia N., Dubrovinsky L. Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain // Acta Crystallographica Section E: Crystallographic Communications. 2018. Vol. 74. No. 10. pp. 1392-1395.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1107/S2056989018012161
UR - https://doi.org/10.1107/S2056989018012161
TI - Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain
T2 - Acta Crystallographica Section E: Crystallographic Communications
AU - Bykov, Maxim
AU - Khandarkhaeva, Saiana
AU - Fedotenko, Timofey
AU - Sedmak, Pavel
AU - Dubrovinskaia, Natalia
AU - Dubrovinsky, Leonid
PY - 2018
DA - 2018/09/07 00:00:00
PB - International Union of Crystallography (IUCr)
SP - 1392-1395
IS - 10
VL - 74
PMID - 30319786
SN - 2056-9890
ER -
Cite this
BibTex
Copy
@article{2018_Bykov,
author = {Maxim Bykov and Saiana Khandarkhaeva and Timofey Fedotenko and Pavel Sedmak and Natalia Dubrovinskaia and Leonid Dubrovinsky},
title = {Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain},
journal = {Acta Crystallographica Section E: Crystallographic Communications},
year = {2018},
volume = {74},
publisher = {International Union of Crystallography (IUCr)},
month = {sep},
url = {https://doi.org/10.1107/S2056989018012161},
number = {10},
pages = {1392--1395},
doi = {10.1107/S2056989018012161}
}
Cite this
MLA
Copy
Bykov, Maxim, et al. “Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain.” Acta Crystallographica Section E: Crystallographic Communications, vol. 74, no. 10, Sep. 2018, pp. 1392-1395. https://doi.org/10.1107/S2056989018012161.
Profiles