Selective Synthesis of γ-WO3 and β-WO3 ⋅H2 O by the Hydrothermal Treatment of Peroxotungstic Acid
T M Bushkova
1
,
A A Egorova
1
,
A V Khoroshilov
1
,
O.S. Ivanova
1
,
A D Yapryntsev
1
,
A E Baranchikov
1
,
Publication type: Journal Article
Publication date: 2021-04-27
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
A selective method has been suggested for the synthesis of highly dispersed powders of γ-WO3 (monoclinic) and β-WO3⋅H2O (orthorhombic) by the hydrothermal treatment of aqueous suspensions of peroxotungstic acid in temperature range 70–250°С. The hydrothermal treatment of suspensions of peroxotungstic acid leads to formation of monophase β-WO3⋅H2O at temperature up to 100°С and monophase γ-WO3 at 250°С. The hydrothermal treatment in the temperature range 120–200°С gives two-phase samples of γ-WO3 and β-WO3⋅0.33H2O (orthorhombic syngony). The obtained monophase and two-phase powders have been studied by X-ray powder diffraction, scanning electron microscopy, IR spectroscopy, thermal analysis, and diffuse reflectance spectroscopy.
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11
Total citations:
11
Citations from 2024:
7
(63%)
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GOST
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Bushkova T. M. et al. Selective Synthesis of γ-WO3 and β-WO3⋅H2O by the Hydrothermal Treatment of Peroxotungstic Acid // Russian Journal of Inorganic Chemistry. 2021. Vol. 66. No. 4. pp. 496-501.
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Bushkova T. M., Egorova A. A., Khoroshilov A. V., Ivanova O., Yapryntsev A. D., Baranchikov A. E., Ivanov V. Selective Synthesis of γ-WO3 and β-WO3⋅H2O by the Hydrothermal Treatment of Peroxotungstic Acid // Russian Journal of Inorganic Chemistry. 2021. Vol. 66. No. 4. pp. 496-501.
Cite this
RIS
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TY - JOUR
DO - 10.1134/S0036023621040070
UR - https://link.springer.com/10.1134/S0036023621040070
TI - Selective Synthesis of γ-WO3 and β-WO3⋅H2O by the Hydrothermal Treatment of Peroxotungstic Acid
T2 - Russian Journal of Inorganic Chemistry
AU - Bushkova, T M
AU - Egorova, A A
AU - Khoroshilov, A V
AU - Ivanova, O.S.
AU - Yapryntsev, A D
AU - Baranchikov, A E
AU - Ivanov, V.K.
PY - 2021
DA - 2021/04/27
PB - Pleiades Publishing
SP - 496-501
IS - 4
VL - 66
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2021_Bushkova,
author = {T M Bushkova and A A Egorova and A V Khoroshilov and O.S. Ivanova and A D Yapryntsev and A E Baranchikov and V.K. Ivanov},
title = {Selective Synthesis of γ-WO3 and β-WO3⋅H2O by the Hydrothermal Treatment of Peroxotungstic Acid},
journal = {Russian Journal of Inorganic Chemistry},
year = {2021},
volume = {66},
publisher = {Pleiades Publishing},
month = {apr},
url = {https://link.springer.com/10.1134/S0036023621040070},
number = {4},
pages = {496--501},
doi = {10.1134/S0036023621040070}
}
Cite this
MLA
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Bushkova, T. M., et al. “Selective Synthesis of γ-WO3 and β-WO3⋅H2O by the Hydrothermal Treatment of Peroxotungstic Acid.” Russian Journal of Inorganic Chemistry, vol. 66, no. 4, Apr. 2021, pp. 496-501. https://link.springer.com/10.1134/S0036023621040070.