Physics of the Solid State

, том 61 , издание 11 , страницы 2200-2217

Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles

V G Ilves ¹

S Yu Sokovnin ^{1, 2}

M.G. Zuev ^{2, 3}

M A Uimin ^{2, 4}

M Rähn ⁵

J Kozlova ⁵

V. Sammelselg ^{5, 6}

Скрыть аффилиации авторов Показать аффилиации авторов: 6 аффилиаций

Institute of Electrophysics, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia |

Ural Federal University named after the First president of Russia B.N. Yeltsin, Yekaterinburg, Russia |

Institute of Solid State Chemistry, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia |

⁴

Mikheev Institute of Metal Physics, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia |

⁵

Institute of Physics, University of Tartu, Tartu, Estonia |

⁶

Institute of Chemistry, University of Tartu, Tartu, Estonia |

Тип публикации: Journal Article

Дата публикации: 2019-11-05

Pleiades Publishing

Physics of the Solid State

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ISSN: 10637834, 10906460, 17267498

DOI: 10.1134/S1063783419110179

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Electronic, Optical and Magnetic Materials

Condensed Matter Physics

Краткое описание

Mesoporous nanocrystalline CaF2 powder was produced by pulsed electron beam evaporation (PEBE) in vacuum. The specific surface area (SSA) of CaF2 nanopowder (NP) reached 88.7 m2/g. The effect of in-air thermal annealing in the temperature range of 200–900°C on the particle size, morphology, textural, thermal, magnetic, and luminescence properties of NPs is studied. A strong deviation from stoichiometry is observed in produced nanoparticles and a significant increase in the SSA after annealing at 200°C. The obtained CaF2 NP shows ferromagnetic (FM) behavior. The FM response appearance can be explained by the formation of structural and radiation defects. An analysis of pulsed cathodoluminescence (PCL) and magnetization curves of CaF2 NPs allows conclusions about their interrelation.

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Ilves V. G. et al. Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles // Physics of the Solid State. 2019. Vol. 61. No. 11. pp. 2200-2217.

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Ilves V. G., Sokovnin S. Yu., Zuev M., Uimin M. A., Rähn M., Kozlova J., Sammelselg V. Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles // Physics of the Solid State. 2019. Vol. 61. No. 11. pp. 2200-2217.

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TY - JOUR

DO - 10.1134/S1063783419110179

UR - https://doi.org/10.1134/S1063783419110179

TI - Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles

T2 - Physics of the Solid State

AU - Ilves, V G

AU - Sokovnin, S Yu

AU - Zuev, M.G.

AU - Uimin, M A

AU - Rähn, M

AU - Kozlova, J

AU - Sammelselg, V.

PY - 2019

DA - 2019/11/05

PB - Pleiades Publishing

SP - 2200-2217

IS - 11

VL - 61

SN - 1063-7834

SN - 1090-6460

SN - 1726-7498

ER -

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@article{2019_Ilves,

author = {V G Ilves and S Yu Sokovnin and M.G. Zuev and M A Uimin and M Rähn and J Kozlova and V. Sammelselg},

title = {Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles},

journal = {Physics of the Solid State},

year = {2019},

volume = {61},

publisher = {Pleiades Publishing},

month = {nov},

url = {https://doi.org/10.1134/S1063783419110179},

number = {11},

pages = {2200--2217},

doi = {10.1134/S1063783419110179}

}

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Ilves, V. G., et al. “Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles.” Physics of the Solid State, vol. 61, no. 11, Nov. 2019, pp. 2200-2217. https://doi.org/10.1134/S1063783419110179.