Physics of the Solid State

, volume 61 , issue 11 , pages 2200-2217

Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles

V G Ilves ¹

S Yu Sokovnin ^{1, 2}

M.G. Zuev ^{2, 3}

M A Uimin ^{2, 4}

M Rähn ⁵

J Kozlova ⁵

V. Sammelselg ^{5, 6}

Hide authors affiliations Show authors affiliations: 6 affiliations

Institute of Electrophysics, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia |

Ural Federal University named after the First president of Russia B.N. Yeltsin, Yekaterinburg, Russia |

Institute of Solid State Chemistry, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia |

⁴

Mikheev Institute of Metal Physics, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia |

⁵

Institute of Physics, University of Tartu, Tartu, Estonia |

⁶

Institute of Chemistry, University of Tartu, Tartu, Estonia |

Publication type: Journal Article

Publication date: 2019-11-05

Pleiades Publishing

Physics of the Solid State

scimago Q4

wos Q3

SJR: 0.183

CiteScore: 1.4

Impact factor: 1.8

ISSN: 10637834, 10906460, 17267498

DOI: 10.1134/S1063783419110179

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Electronic, Optical and Magnetic Materials

Condensed Matter Physics

Abstract

Mesoporous nanocrystalline CaF2 powder was produced by pulsed electron beam evaporation (PEBE) in vacuum. The specific surface area (SSA) of CaF2 nanopowder (NP) reached 88.7 m2/g. The effect of in-air thermal annealing in the temperature range of 200–900°C on the particle size, morphology, textural, thermal, magnetic, and luminescence properties of NPs is studied. A strong deviation from stoichiometry is observed in produced nanoparticles and a significant increase in the SSA after annealing at 200°C. The obtained CaF2 NP shows ferromagnetic (FM) behavior. The FM response appearance can be explained by the formation of structural and radiation defects. An analysis of pulsed cathodoluminescence (PCL) and magnetization curves of CaF2 NPs allows conclusions about their interrelation.

Found

3 citations

Uimin Mikhail

PhD in Physics and Mathematics

180 publications, 2 060 citations

h-index: 23

M.N. Mikheev Institute of Metal Physics of the Ural Branch of the Russian Academy of Sciences

1 citation

Korusenko Petr

🥼 🤝

PhD in Physics and Mathematics

83 publications, 643 citations, 23 reviews

h-index: 14

Saint Petersburg State University

Omsk State Technical University

National Research Nuclear University MEPhI

Research interests

Photoelectron spectroscopy

X-ray spectroscopy

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GOST |

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Ilves V. G. et al. Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles // Physics of the Solid State. 2019. Vol. 61. No. 11. pp. 2200-2217.

GOST all authors (up to 50) Copy

Ilves V. G., Sokovnin S. Yu., Zuev M., Uimin M. A., Rähn M., Kozlova J., Sammelselg V. Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles // Physics of the Solid State. 2019. Vol. 61. No. 11. pp. 2200-2217.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1134/S1063783419110179

UR - https://doi.org/10.1134/S1063783419110179

TI - Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles

T2 - Physics of the Solid State

AU - Ilves, V G

AU - Sokovnin, S Yu

AU - Zuev, M.G.

AU - Uimin, M A

AU - Rähn, M

AU - Kozlova, J

AU - Sammelselg, V.

PY - 2019

DA - 2019/11/05

PB - Pleiades Publishing

SP - 2200-2217

IS - 11

VL - 61

SN - 1063-7834

SN - 1090-6460

SN - 1726-7498

ER -

BibTex |

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BibTex (up to 50 authors) Copy

@article{2019_Ilves,

author = {V G Ilves and S Yu Sokovnin and M.G. Zuev and M A Uimin and M Rähn and J Kozlova and V. Sammelselg},

title = {Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles},

journal = {Physics of the Solid State},

year = {2019},

volume = {61},

publisher = {Pleiades Publishing},

month = {nov},

url = {https://doi.org/10.1134/S1063783419110179},

number = {11},

pages = {2200--2217},

doi = {10.1134/S1063783419110179}

}

MLA

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MLA Copy

Ilves, V. G., et al. “Effect of Annealing on Structural, Textural, Thermal, Magnetic, and Luminescence Properties of Calcium Fluoride Nanoparticles.” Physics of the Solid State, vol. 61, no. 11, Nov. 2019, pp. 2200-2217. https://doi.org/10.1134/S1063783419110179.

Publisher

Pleiades Publishing

Journal

Physics of the Solid State

scimago Q4

wos Q3

SJR

0.183

CiteScore

1.4

Impact factor

1.8

ISSN

10637834 (Print)

10906460 (Electronic)

17267498 (Print)

Labs

Laboratory of Applied Magnetism

Profiles

Mikhail A Uimin