Open Access
Crystallization of Nano-Sized Macromolecules by the Example of Hexakis-[4-{(N-Allylimino)methyl}phenoxy]cyclotriphosphazene
Publication type: Journal Article
Publication date: 2022-06-30
PubMed ID:
35808103
General Chemical Engineering
General Materials Science
Abstract
The synthesized compound was characterized by 31P, 13C, and 1H NMR spectroscopy and MALDI-TOF mass spectroscopy. According to DSC data, the compound was initially crystalline, but the crystal structure was defective. The crystals suitable for X-ray diffraction study were prepared by slow precipitation of the compound from a solution by a vapor of another solvent. A study of the single crystal obtained in this way demonstrated that the phosphazene ring has a flattened chair conformation. It was found that the sphere circumscribed around the compound molecule has a diameter of 2.382 nm.
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Chistyakov E., Yudaev P., Nelyubina Y. V. Crystallization of Nano-Sized Macromolecules by the Example of Hexakis-[4-{(N-Allylimino)methyl}phenoxy]cyclotriphosphazene // Nanomaterials. 2022. Vol. 12. No. 13. p. 2268.
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Chistyakov E., Yudaev P., Nelyubina Y. V. Crystallization of Nano-Sized Macromolecules by the Example of Hexakis-[4-{(N-Allylimino)methyl}phenoxy]cyclotriphosphazene // Nanomaterials. 2022. Vol. 12. No. 13. p. 2268.
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RIS
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TY - JOUR
DO - 10.3390/nano12132268
UR - https://www.mdpi.com/2079-4991/12/13/2268
TI - Crystallization of Nano-Sized Macromolecules by the Example of Hexakis-[4-{(N-Allylimino)methyl}phenoxy]cyclotriphosphazene
T2 - Nanomaterials
AU - Chistyakov, Evgeniy
AU - Yudaev, Pavel
AU - Nelyubina, Yulia V.
PY - 2022
DA - 2022/06/30
PB - MDPI
SP - 2268
IS - 13
VL - 12
PMID - 35808103
SN - 2079-4991
ER -
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BibTex (up to 50 authors)
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@article{2022_Chistyakov,
author = {Evgeniy Chistyakov and Pavel Yudaev and Yulia V. Nelyubina},
title = {Crystallization of Nano-Sized Macromolecules by the Example of Hexakis-[4-{(N-Allylimino)methyl}phenoxy]cyclotriphosphazene},
journal = {Nanomaterials},
year = {2022},
volume = {12},
publisher = {MDPI},
month = {jun},
url = {https://www.mdpi.com/2079-4991/12/13/2268},
number = {13},
pages = {2268},
doi = {10.3390/nano12132268}
}
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MLA
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Chistyakov, Evgeniy, et al. “Crystallization of Nano-Sized Macromolecules by the Example of Hexakis-[4-{(N-Allylimino)methyl}phenoxy]cyclotriphosphazene.” Nanomaterials, vol. 12, no. 13, Jun. 2022, p. 2268. https://www.mdpi.com/2079-4991/12/13/2268.
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