Mendeleev Communications, volume 20, issue 4, pages 212-214
Unexpected formation of 5,5-diethoxy-5H-1,2,3-dithiazoles from 5H-1,2,3-dithiazole-5-thiones
Publication type: Journal Article
Publication date: 2010-07-11
Journal:
Mendeleev Communications
Quartile SCImago
Q3
Quartile WOS
Q3
Impact factor: 1.9
ISSN: 09599436, 1364551X
General Chemistry
Abstract
(no carbonsignals in the region 160–220 ppm).Careful investigation of this reaction showed that the bestyield was achieved when 5-fold excess of sodium ethoxide wasused (55% yield). Note that this amount significantly exceededthe required quantity of the reagent (one or two equivalents).However, when less amount of the reagent was used, some ofthe starting thione
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Bol'shakov O. et al. Unexpected formation of 5,5-diethoxy-5H-1,2,3-dithiazoles from 5H-1,2,3-dithiazole-5-thiones // Mendeleev Communications. 2010. Vol. 20. No. 4. pp. 212-214.
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Bol'shakov O., Konstantinova L. S., Aysin R., Obruchnikova N. V., Lubuzh E. D., Rakitin O. A. Unexpected formation of 5,5-diethoxy-5H-1,2,3-dithiazoles from 5H-1,2,3-dithiazole-5-thiones // Mendeleev Communications. 2010. Vol. 20. No. 4. pp. 212-214.
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TY - JOUR
DO - 10.1016/j.mencom.2010.06.010
UR - https://doi.org/10.1016%2Fj.mencom.2010.06.010
TI - Unexpected formation of 5,5-diethoxy-5H-1,2,3-dithiazoles from 5H-1,2,3-dithiazole-5-thiones
T2 - Mendeleev Communications
AU - Bol'shakov, Oleg
AU - Konstantinova, Lidia S.
AU - Aysin, Rinat
AU - Obruchnikova, Natalia V.
AU - Lubuzh, Elena D
AU - Rakitin, Oleg A.
PY - 2010
DA - 2010/07/11 00:00:00
PB - Elsevier
SP - 212-214
IS - 4
VL - 20
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2010_Bol'shakov,
author = {Oleg Bol'shakov and Lidia S. Konstantinova and Rinat Aysin and Natalia V. Obruchnikova and Elena D Lubuzh and Oleg A. Rakitin},
title = {Unexpected formation of 5,5-diethoxy-5H-1,2,3-dithiazoles from 5H-1,2,3-dithiazole-5-thiones},
journal = {Mendeleev Communications},
year = {2010},
volume = {20},
publisher = {Elsevier},
month = {jul},
url = {https://doi.org/10.1016%2Fj.mencom.2010.06.010},
number = {4},
pages = {212--214},
doi = {10.1016/j.mencom.2010.06.010}
}
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MLA
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Bol'shakov, Oleg, et al. “Unexpected formation of 5,5-diethoxy-5H-1,2,3-dithiazoles from 5H-1,2,3-dithiazole-5-thiones.” Mendeleev Communications, vol. 20, no. 4, Jul. 2010, pp. 212-214. https://doi.org/10.1016%2Fj.mencom.2010.06.010.