Applied Surface Science, volume 258, issue 7, pages 3168-3172
Anhydride modified silica nanoparticles: Preparation and characterization
Barabanova A. I.
1
,
Zavin B G
1
,
Vygodskii Ya.S.
1
,
Philippova O E
,
Askadskii A A
1
,
Afanasev E S
1
,
Pryakhina T.A.
1
,
Philippova O.E.
2
,
Publication type: Journal Article
Publication date: 2012-01-01
Journal:
Applied Surface Science
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 6.7
ISSN: 01694332
Surfaces, Coatings and Films
General Chemistry
General Physics and Astronomy
Condensed Matter Physics
Surfaces and Interfaces
Abstract
a b s t r a c t The paper describes modification of colloid silica nanoparticles, using 3-(triethoxysilyl)propylsuccinic anhydride (TESPSA) as a reagent. Anhydride groups were grafted to the silica surface by an interaction of the surface silanol Si-OH groups with reactive ethoxy groups of TESPSA. Elemental analysis, FTIR and 1 H NMR spectroscopy were employed to characterize silica nanoparticles before and after surface modification. It was demonstrated that only fifty percent of silica surface silanol groups are involved in the reaction with TESPSA. Size distribution of nanoparticles determined by atomic force microscopy (AFM) technique shows that nanoparticles preserve their size upon modification. TESPSA-modified silica nanoparticles can be used as polyfunctional curing agent for epoxy resin.
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1 publication, 3.03%
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1
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Citations by publishers
2
4
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12
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3 publications, 9.09%
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3 publications, 9.09%
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3 publications, 9.09%
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1 publication, 3.03%
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1 publication, 3.03%
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1 publication, 3.03%
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1 publication, 3.03%
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2
4
6
8
10
12
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- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Barabanova A. I. et al. Anhydride modified silica nanoparticles: Preparation and characterization // Applied Surface Science. 2012. Vol. 258. No. 7. pp. 3168-3172.
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Barabanova A. I., Pryakhina T., Afanasev E. S., Zavin B. G., Vygodskii Y., Askadskii A. A., Philippova O. E., Khokhlov A. R., Philippova O., Khokhlov A. R. Anhydride modified silica nanoparticles: Preparation and characterization // Applied Surface Science. 2012. Vol. 258. No. 7. pp. 3168-3172.
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TY - JOUR
DO - 10.1016/j.apsusc.2011.11.057
UR - https://doi.org/10.1016%2Fj.apsusc.2011.11.057
TI - Anhydride modified silica nanoparticles: Preparation and characterization
T2 - Applied Surface Science
AU - Barabanova, A. I.
AU - Pryakhina, T.A.
AU - Afanasev, E S
AU - Zavin, B G
AU - Vygodskii, Ya.S.
AU - Askadskii, A A
AU - Philippova, O E
AU - Khokhlov, A R
AU - Philippova, O.E.
AU - Khokhlov, Alexei R.
PY - 2012
DA - 2012/01/01 00:00:00
PB - Elsevier
SP - 3168-3172
IS - 7
VL - 258
SN - 0169-4332
ER -
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@article{2012_Barabanova,
author = {A. I. Barabanova and T.A. Pryakhina and E S Afanasev and B G Zavin and Ya.S. Vygodskii and A A Askadskii and O E Philippova and A R Khokhlov and O.E. Philippova and Alexei R. Khokhlov},
title = {Anhydride modified silica nanoparticles: Preparation and characterization},
journal = {Applied Surface Science},
year = {2012},
volume = {258},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016%2Fj.apsusc.2011.11.057},
number = {7},
pages = {3168--3172},
doi = {10.1016/j.apsusc.2011.11.057}
}
Cite this
MLA
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Barabanova, A. I., et al. “Anhydride modified silica nanoparticles: Preparation and characterization.” Applied Surface Science, vol. 258, no. 7, Jan. 2012, pp. 3168-3172. https://doi.org/10.1016%2Fj.apsusc.2011.11.057.
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