First metallacarborane ethene complex [1,8-Me2-2,2-(C2H4)2-7-SMe2-2,1,8-IrC2B9H8] and its reaction with iodine
Publication type: Journal Article
Publication date: 2016-03-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Metallacarborane [1,8-Me2-2,2-(C2H4)2-7-SMe2-2,1,8-IrC2B9H8] (1) was obtained by an interaction of [(C2H4)2IrCl]2 with Tl[9-SMe2-7,8-Me2-7,8-C2B9H8]. Reaction proceeds with a low temperature “1,2 → 1,7” polyhedral rearrangement. Ethene complex 1 reacts with iodine in toluene with the formation of ionic compound 3, consisting of cationic [(1,8-Me2-7-SMe2-2,1,8-IrC2B9H8)2I3]+ (3a+) and anionic [(1,8-Me2-7-SMe-2,1,8-IrC2B9H8)2I3]− (3b–) iodide species. The structures of 1 and 3 were determined by X-ray diffraction.
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Vinogradov M. M. et al. First metallacarborane ethene complex [1,8-Me2-2,2-(C2H4)2-7-SMe2-2,1,8-IrC2B9H8] and its reaction with iodine // Journal of Organometallic Chemistry. 2016. Vol. 805. pp. 54-58.
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Vinogradov M. M., Nelyubina Y. V., Ikonnikov N. S., Strelkova T. V., Kudinov A. R. First metallacarborane ethene complex [1,8-Me2-2,2-(C2H4)2-7-SMe2-2,1,8-IrC2B9H8] and its reaction with iodine // Journal of Organometallic Chemistry. 2016. Vol. 805. pp. 54-58.
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TY - JOUR
DO - 10.1016/j.jorganchem.2015.12.022
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X15302369
TI - First metallacarborane ethene complex [1,8-Me2-2,2-(C2H4)2-7-SMe2-2,1,8-IrC2B9H8] and its reaction with iodine
T2 - Journal of Organometallic Chemistry
AU - Vinogradov, Mikhail M
AU - Nelyubina, Yulia V.
AU - Ikonnikov, Nikolay S
AU - Strelkova, Tatyana V.
AU - Kudinov, Alexander R
PY - 2016
DA - 2016/03/01
PB - Elsevier
SP - 54-58
VL - 805
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2016_Vinogradov,
author = {Mikhail M Vinogradov and Yulia V. Nelyubina and Nikolay S Ikonnikov and Tatyana V. Strelkova and Alexander R Kudinov},
title = {First metallacarborane ethene complex [1,8-Me2-2,2-(C2H4)2-7-SMe2-2,1,8-IrC2B9H8] and its reaction with iodine},
journal = {Journal of Organometallic Chemistry},
year = {2016},
volume = {805},
publisher = {Elsevier},
month = {mar},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X15302369},
pages = {54--58},
doi = {10.1016/j.jorganchem.2015.12.022}
}
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