Air-Stable Arene Manganese Complexes as Catalysts for the Syngas-Assisted Direct Reductive Amination, Cyanation of Aldehyde, and CO2 Fixation by Epoxide with High Functional Groups Tolerance
Ivan V. Smirnov
1, 2
,
Klim O Biriukov
1
,
Klim Olegovich Biriukov
1
,
Dmitry S Perekalin
1, 2
,
Oleg I Afanasyev
1, 3
,
Denis Chusov
1, 2
Publication type: Journal Article
Publication date: 2024-06-29
scimago Q2
wos Q1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
PubMed ID:
38943599
Abstract
Manganese complexes [(arene)Mn(CO)3]+ were prepared in one step from arenes and Mn(CO)5Br. They were found to be efficient catalysts in the carbonyl cyanation with TMSCN, CO2 fixation by epoxides, and direct reductive amination in the presence of syngas. The amination reaction tolerated various reducible functional groups. The synergy of carbon monoxide and hydrogen in syngas provides high efficiency of the catalytic system. The developed protocols do not require an inert atmosphere, and the catalysts can be handled in air.
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Smirnov I. V. et al. Air-Stable Arene Manganese Complexes as Catalysts for the Syngas-Assisted Direct Reductive Amination, Cyanation of Aldehyde, and CO2 Fixation by Epoxide with High Functional Groups Tolerance // Journal of Organic Chemistry. 2024. Vol. 89. No. 14. pp. 10338-10343.
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Smirnov I. V., Biriukov K. O., Biriukov K. O., Shvydkiy N. V., Perekalin D. S., Afanasyev O. I., Chusov D. Air-Stable Arene Manganese Complexes as Catalysts for the Syngas-Assisted Direct Reductive Amination, Cyanation of Aldehyde, and CO2 Fixation by Epoxide with High Functional Groups Tolerance // Journal of Organic Chemistry. 2024. Vol. 89. No. 14. pp. 10338-10343.
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TY - JOUR
DO - 10.1021/acs.joc.4c00842
UR - https://pubs.acs.org/doi/10.1021/acs.joc.4c00842
TI - Air-Stable Arene Manganese Complexes as Catalysts for the Syngas-Assisted Direct Reductive Amination, Cyanation of Aldehyde, and CO2 Fixation by Epoxide with High Functional Groups Tolerance
T2 - Journal of Organic Chemistry
AU - Smirnov, Ivan V.
AU - Biriukov, Klim O
AU - Biriukov, Klim Olegovich
AU - Shvydkiy, Nikita V
AU - Perekalin, Dmitry S
AU - Afanasyev, Oleg I
AU - Chusov, Denis
PY - 2024
DA - 2024/06/29
PB - American Chemical Society (ACS)
SP - 10338-10343
IS - 14
VL - 89
PMID - 38943599
SN - 0022-3263
SN - 1520-6904
ER -
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BibTex (up to 50 authors)
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@article{2024_Smirnov,
author = {Ivan V. Smirnov and Klim O Biriukov and Klim Olegovich Biriukov and Nikita V Shvydkiy and Dmitry S Perekalin and Oleg I Afanasyev and Denis Chusov},
title = {Air-Stable Arene Manganese Complexes as Catalysts for the Syngas-Assisted Direct Reductive Amination, Cyanation of Aldehyde, and CO2 Fixation by Epoxide with High Functional Groups Tolerance},
journal = {Journal of Organic Chemistry},
year = {2024},
volume = {89},
publisher = {American Chemical Society (ACS)},
month = {jun},
url = {https://pubs.acs.org/doi/10.1021/acs.joc.4c00842},
number = {14},
pages = {10338--10343},
doi = {10.1021/acs.joc.4c00842}
}
Cite this
MLA
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Smirnov, Ivan V., et al. “Air-Stable Arene Manganese Complexes as Catalysts for the Syngas-Assisted Direct Reductive Amination, Cyanation of Aldehyde, and CO2 Fixation by Epoxide with High Functional Groups Tolerance.” Journal of Organic Chemistry, vol. 89, no. 14, Jun. 2024, pp. 10338-10343. https://pubs.acs.org/doi/10.1021/acs.joc.4c00842.