Tris(pyrazolyl)borate rhodium complexes. Application for reductive amination and esterification of aldehydes in the presence of carbon monoxide
Vladimir S Ostrovskii
1
,
Denis Chusov
1
,
Publication type: Journal Article
Publication date: 2020-10-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The halide complexes TpRhCl 2 (MeOH) and Tp Me2 RhI 2 (CO) (Tp = hydrotris-(pyrazolyl)borate; Tp Me2 = hydrotris-(3,5-dimethylpyrazolyl)borate) were synthesized by reactions of RhCl 3 with K[Tp] in methanol and Tp Me2 Rh(CO) 2 with iodine, respectively. Reactions of Tp Me2 RhCl 2 (MeOH) and Tp Me2 RhI 2 (CO) with 1,10-phenanthroline afford the phenanthroline derivatives [Tp Me2 Rh(phen)X] + (X = Cl, I). The structures of TpRhCl 2 (MeOH) and TpRhI 2 (CO) were determined by X-ray diffraction. Tris(pyrazolyl)borate rhodium complexes effectively catalyze the reductive amination and the reductive esterification of aldehydes in the presence of carbon monoxide.
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Kharitonov V. L. et al. Tris(pyrazolyl)borate rhodium complexes. Application for reductive amination and esterification of aldehydes in the presence of carbon monoxide // Journal of Organometallic Chemistry. 2020. Vol. 925. p. 121468.
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Kharitonov V. L., Ostrovskii V. S., Nelyubina Y. V., Muratov D. S., Chusov D., Loginov D. A. Tris(pyrazolyl)borate rhodium complexes. Application for reductive amination and esterification of aldehydes in the presence of carbon monoxide // Journal of Organometallic Chemistry. 2020. Vol. 925. p. 121468.
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TY - JOUR
DO - 10.1016/j.jorganchem.2020.121468
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X20303703
TI - Tris(pyrazolyl)borate rhodium complexes. Application for reductive amination and esterification of aldehydes in the presence of carbon monoxide
T2 - Journal of Organometallic Chemistry
AU - Kharitonov, Vladimir L.
AU - Ostrovskii, Vladimir S
AU - Nelyubina, Yulia V.
AU - Muratov, Dmitry S.
AU - Chusov, Denis
AU - Loginov, Dmitry A.
PY - 2020
DA - 2020/10/01
PB - Elsevier
SP - 121468
VL - 925
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2020_Kharitonov,
author = {Vladimir L. Kharitonov and Vladimir S Ostrovskii and Yulia V. Nelyubina and Dmitry S. Muratov and Denis Chusov and Dmitry A. Loginov},
title = {Tris(pyrazolyl)borate rhodium complexes. Application for reductive amination and esterification of aldehydes in the presence of carbon monoxide},
journal = {Journal of Organometallic Chemistry},
year = {2020},
volume = {925},
publisher = {Elsevier},
month = {oct},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X20303703},
pages = {121468},
doi = {10.1016/j.jorganchem.2020.121468}
}